N-(3-溴丙基)苯二胺合成路线 （共 93 条）
反应条件
[Ni0(1,5-cyclooctadiene)2]; zinc; (4-Cl)-H-PyBox in N,N-dimethyl acetamide T=25°C; 3 h; Inert atmosphere;
参考文献
Yu, Xiaolong; Yang, Tao; Wang, Shulin; Xu, Hailiang; Gong, Hegui
Organic Letters, 2011 , vol. 13, # 8 p. 2138 - 2141
反应条件
potassium carbonate in acetonitrile 0.1 h; Heatingmicrowave irradiation;
参考文献
He, Ling; Li, Ju-Lian; Zhang, Jian-Jun; Su, Pu; Zheng, Shi-Long
Synthetic Communications, 2003 , vol. 33, # 5 p. 741 - 747
参考文献
Manske; Perkin; Robinson
Journal of the Chemical Society, 1927 , p. 7
Full Text Show Details
Gabriel
Chemische Berichte, 1909 , vol. 42, p. 1241
参考文献
Andersen, Knud Erik; Dorwald, Florencio Zaragiza; Peschke, Bernd; Sidelmann, Ulla Grove; Rudolf, Klaus; Stenkamp, Dirk; Hurnaus, Rudolf; Muller, Stephan Georg; Krist, Bernd; Eriksen, Birgitte
Patent: US2002/58659 A1, 2002 ;
US 20020058659 A1
反应条件
acetic acid; sodium nitrite in dimethyl sulfoxide T=35°C;
参考文献
Matt, Christophe; Wagner, Alain; Mioskowski, Charles
Journal of Organic Chemistry, 1997 , vol. 62, # 2 p. 234 - 235
反应条件
water; sodium sulfite anschliessend Behandeln mit wss.NaOH;
参考文献
Rumpf
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1937 , vol. 204, p. 593
Bulletin de la Societe Chimique de France, 1938 , vol. <5>5, p. 884
反应条件
anschliessend mit wss. Natronlauge;
参考文献
Rumpf
Bulletin de la Societe Chimique de France, 1938 , vol. <5>5, p. 871,875
反应条件
(i) KOH, MeOH, (ii) aq. KOH, (heating); Multistep reaction;
参考文献
Ledochowski,A. et al.
Roczniki Chemii, 1969 , vol. 43, # 5 p. 1083 - 1087
反应条件
methanol; sodium hydrogensulfide Erwaermen des Reaktionsprodukts mit Hydrazin-hydrat in Aethanol;
参考文献
Bergmann; Kaluszyner
Recueil des Travaux Chimiques des Pays-Bas, 1959 , vol. 78, p. 289,309
反应条件
hydrogen bromide; acetic acid
参考文献
Hamer; Rathbone
Journal of the Chemical Society, 1943 , p. 243,247
