N-苯甲酰基-N'-(4-羟基苯基)硫脲合成路线 （共 5 条）
反应条件
sodium hydroxide T=75 - 80°C; 0.333333 h;
参考文献
Rasmussen, C. R.; Villani, F. J.; Weaner, L. E.; Reynolds, B. E.; Hood, A. R.; et al.
Synthesis, 1988 , # 6 p. 456 - 459
反应条件
1: 65 percent / 10 percent NaOH / 2 h / 90 °C 2: 91 percent / methanol / 4 h / Heating 3: 75 percent / ethanol / 16 h 4: 84 percent / K2CO3 / dimethylformamide / 12 h / 70 °C View Scheme
参考文献
Agarwal, Shiv K.; Saxena, Anil K.; Jain, Padam C.; Sur, R. N.; Srimal, Rikhab C.; et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 642 - 646
反应条件
in acetone
0.5 h; Heating;
参考文献
Rasmussen, C. R.; Villani, F. J.; Weaner, L. E.; Reynolds, B. E.; Hood, A. R.; et al.
Synthesis, 1988 , # 6 p. 456 - 459
反应条件
1: ammonium thiocyanate; benzoyl chloride With PEG-400 in dichloromethane
T=20°C; 1 h;
2: 4-amino-phenol in dichloromethane
2 h;
参考文献
Zhang; Wei; Gao
Synthetic Communications, 2001 , vol. 31, # 20 p. 3099 - 3105
反应条件
1: SiO2 / 1,2-dichloro-ethane / 2 h / 25 °C
2: 1,2-dichloro-ethane / 1 h / 25 °C
View Scheme
参考文献
Kodomari, Mitsuo; Suzuki, Masato; Tanigawa, Keiko; Aoyama, Tadashi
Tetrahedron Letters, 2005 , vol. 46, # 35 p. 5841 - 5843
