1-(3-溴苯基)环丙烷胺合成路线 （共 4 条）
反应条件
1: With diphenyl phosphoryl azide; triethylamine in N,N-dimethyl-formamide T=20 - 100°C; 18 h; 2: With hydrogenchloride in water; N,N-dimethyl-formamide
参考文献
Boehringer Ingelheim International GmbH
Patent: US2006/116370 A1, 2006 ;
Location in patent: Page/Page column 7 ;
反应条件
titanium(IV) isopropylate; boron trifluoride diethyl etherate in diethyl ether T=-70 - 20°C; 2.16667 h;
参考文献
Bertus, Philippe; Szymoniak, Jan
Journal of Organic Chemistry, 2003 , vol. 68, # 18 p. 7133 - 7136
反应条件
sodium carbonate in water
参考文献
WO2004/821 A1, ;
Page 29; 30 ;
反应条件
1: With hydrogenchloride; water in 1,4-dioxane 2 h; 2: With sodium hydroxide in water
参考文献
WO2005/95326 A2, ;
Page/Page column 232-233 ;
WO 2005/095326 A2
