1,3,5-戊烷三羧酸三甲酯合成路线 （共 4 条）
反应条件
sulfuric acid; 1,2-dichloro-ethane
unter Entfernen des gebildeten Wassers;
参考文献
Koehler et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 5779,5782
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Sengupta
Journal of Organic Chemistry, 1953 , vol. 18, p. 249,253
反应条件
1: concentrated aqueous hydrochloric acid
2: 1,2-dichloro-ethane; sulfuric acid / unter Entfernen des gebildeten Wassers
View Scheme
参考文献
Koehler et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 5779,5782
反应条件
1: aq. HCl / Heating
2: H2SO4 / benzene / Heating
View Scheme
参考文献
Augustine,R.L.; Bellina,R.F.
Journal of Organic Chemistry, 1969 , vol. 34, # 7 p. 2141 - 2145
反应条件
(i) O3, O2, MeOH, CH2Cl2, (ii) aq. H2O2, (iii) /BRN= 102415/, Et2O; Multistep reaction;
参考文献
Critch,S.C.; Fallis,A.G.
Canadian Journal of Chemistry, 1977 , vol. 55, p. 2845 - 2851
