(2-氨基-2-氧代乙基)磷酸二乙酯合成路线 (共 7 条)
反应条件
potassium hydroxide in benzene T=20°C; Horner-Wadsworth-Emmons reaction; 1 h;
参考文献
Petrova, Jordanka; Momchilova, Snezhana; Vassilev, Nikolay G.
Phosphorus, Sulfur and Silicon and Related Elements, 2000 , vol. 164, p. 87 - 94
反应条件
potassium hydroxide in benzene T=20°C; Horner-Wadsworth-Emmons reaction; 1 h;
参考文献
Petrova, Jordanka; Momchilova, Snezhana; Vassilev, Nikolay G.
Phosphorus, Sulfur and Silicon and Related Elements, 2000 , vol. 164, p. 87 - 94
反应条件
T=150°C; 8 h; Inert atmosphere;
参考文献
Zhang, Jianmin; Polishchuk, Elena A.; Chen, Jie; Ciufolini, Marco A.
Journal of Organic Chemistry, 2009 , vol. 74, # 23 p. 9140 - 9151
参考文献
Nylen
Chemische Berichte, 1924 , vol. 57, p. 1030
Chemische Berichte, 1926 , vol. 59, p. 1120
反应条件
Michaelis-Arbuzov reaction; 0.0166667 h; microwave irradiation;
参考文献
Kiddle, James J.; Gurley, Alison F.
Phosphorus, Sulfur and Silicon and Related Elements, 2000 , vol. 160, p. 195 - 205
反应条件
T=25°C; bei 10-taegigem Stehenlassen;
参考文献
Nylen
Chemische Berichte, 1924 , vol. 57, p. 1030
Chemische Berichte, 1926 , vol. 59, p. 1120
反应条件
hydrogenchloride; dimethylsulfide borane complex
1.) THF, 0 deg C, 1 h then reflux, 3 h; Multistep reaction;
参考文献
Wasielewski, Czeslaw; Dembkowski, Leszek; Topolski, Marek
Synthesis, 1989 , # 1 p. 52 - 53