2-氯-4-甲基-6-硝基苯胺合成路线 （共 6 条）
反应条件
1: With sulfuric acid; sodium nitrite in ethanol T=0 - 20°C; 0.5 h; 2: in ethanol; water Heating; Further stages.;
参考文献
Grella; Danso-Danquah; Safo; Joshi; Kister; Marden; Hoffman; Abraham
Journal of Medicinal Chemistry, 2000 , vol. 43, # 25 p. 4726 - 4737
反应条件
1.1: sulfuric acid; aq. sodium nitrite / ethanol / 0.5 h / 0 - 20 °C 1.2: 69 percent / ethanol; H2O / Heating 2.1: 93 percent / tin(II) chloride dihydrate / ethanol / 3 h / Heating View Scheme
参考文献
Grella; Danso-Danquah; Safo; Joshi; Kister; Marden; Hoffman; Abraham
Journal of Medicinal Chemistry, 2000 , vol. 43, # 25 p. 4726 - 4737
反应条件
N-chloro-succinimide in acetonitrile
Heating;
参考文献
Grella; Danso-Danquah; Safo; Joshi; Kister; Marden; Hoffman; Abraham
Journal of Medicinal Chemistry, 2000 , vol. 43, # 25 p. 4726 - 4737
反应条件
4-nitro-4-methyl-2,3,5,6-tetrabromo-2,5-cyclohexadien-1-one in trifluoroacetic acid
3 h; Ambient temperature;
参考文献
Lemaire, M.; Guy, A.; Boutin, P.; Guette, J. P.
Synthesis, 1989 , # 10 p. 761 - 763
反应条件
nitric acid
T=20°C; man verseift das Acetylderivat mit Schwefelsaeure;
参考文献
Claus; Davidsen
Justus Liebigs Annalen der Chemie, 1891 , vol. 265, p. 343
反应条件
und Verseifung des Reaktionsproduktes mit Schwefelsaeure;
参考文献
Claus; Davidsen
Justus Liebigs Annalen der Chemie, 1891 , vol. 265, p. 343
