4′-氯-3′-硝基苯乙酮合成路线 (共 32 条)
反应条件
in isopropyl alcohol 8 h; Heating;
参考文献
Varma, Rajendra S; Sarin, Simi; Chatterjee, R K
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 10 p. 711 - 713
反应条件
isobutyramide; copper T=100°C; 8 h;
参考文献
Journal of Fluorine Chemistry, , vol. 50, # 3 p. 411 - 426
反应条件
1: 95 percent / K2CO3; Pd(PPh3)4 / toluene; H2O / 18 h / Heating 2: 81 percent / PPh3 / 1,2-dichloro-benzene / 6.5 h / Heating View Scheme
参考文献
Freeman, Adam W.; Urvoy, Marie; Criswell, Megan E.
Journal of Organic Chemistry, 2005 , vol. 70, # 13 p. 5014 - 5019
反应条件
1: 60 percent / NaHCO3 / aq. ethanol / 2 h / Heating
2: 55 percent / FeSO4*7H2O / aq. NH3 / 1 h / Heating
View Scheme
参考文献
Shridhar, D. R.; Sastry, C. V. Reddy; Bansal, O. P.; Rao, Pulla; Singh, P. P.; et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 12 p. 1236 - 1242
反应条件
1: 60 percent / NaHCO3 / aq. ethanol / 2 h / Heating
2: 55 percent / FeSO4*7H2O / aq. NH3 / 1 h / Heating
3: 86 percent / KOH / acetone / 5 h / Heating
4: 70 percent / NH2OH*HCl, pyridine / ethanol / 2 h / Heating
View Scheme
参考文献
Shridhar, D. R.; Sastry, C. V. Reddy; Bansal, O. P.; Rao, Pulla; Singh, P. P.; et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 12 p. 1236 - 1242
反应条件
1: 60 percent / NaHCO3 / aq. ethanol / 2 h / Heating
2: 55 percent / FeSO4*7H2O / aq. NH3 / 1 h / Heating
3: 85 percent / KOH / acetone / 5 h / Heating
4: 76 percent / NH2OH*HCl, pyridine / ethanol / 2 h / Heating
5: 86 percent / aq.NaOH / tetrabutylammonium hydrogen sulphate / 0.5 h / Ambient temperature
View Scheme
参考文献
Shridhar, D. R.; Sastry, C. V. Reddy; Bansal, O. P.; Rao, Pulla; Singh, P. P.; et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 12 p. 1236 - 1242
反应条件
1: 60 percent / NaHCO3 / aq. ethanol / 2 h / Heating
2: 55 percent / FeSO4*7H2O / aq. NH3 / 1 h / Heating
3: 85 percent / KOH / acetone / 5 h / Heating
4: 76 percent / NH2OH*HCl, pyridine / ethanol / 2 h / Heating
5: 93 percent / aq.NaOH / tetrabutylammonium hydrogen sulphate / 0.5 h / Ambient temperature
View Scheme
参考文献
Shridhar, D. R.; Sastry, C. V. Reddy; Bansal, O. P.; Rao, Pulla; Singh, P. P.; et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 12 p. 1236 - 1242
反应条件
1: 60 percent / NaHCO3 / aq. ethanol / 2 h / Heating
2: 55 percent / FeSO4*7H2O / aq. NH3 / 1 h / Heating
3: 86 percent / KOH / acetone / 5 h / Heating
4: 70 percent / NH2OH*HCl, pyridine / ethanol / 2 h / Heating
5: 79 percent / aq.NaOH / tetrabutylammonium hydrogen sulphate / 0.5 h / Ambient temperature
View Scheme
参考文献
Shridhar, D. R.; Sastry, C. V. Reddy; Bansal, O. P.; Rao, Pulla; Singh, P. P.; et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 12 p. 1236 - 1242
反应条件
1: 60 percent / NaHCO3 / aq. ethanol / 2 h / Heating
2: 55 percent / FeSO4*7H2O / aq. NH3 / 1 h / Heating
3: 86 percent / KOH / acetone / 5 h / Heating
4: 70 percent / NH2OH*HCl, pyridine / ethanol / 2 h / Heating
5: 78 percent / aq.NaOH / tetrabutylammonium hydrogen sulphate / 0.5 h / Ambient temperature
6: 85 percent / aq.NaOH / 2 h / Heating
7: 80 percent / Et3N / dimethylformamide / 2 h / Heating
View Scheme
参考文献
Shridhar, D. R.; Sastry, C. V. Reddy; Bansal, O. P.; Rao, Pulla; Singh, P. P.; et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 12 p. 1236 - 1242
反应条件
1: 60 percent / NaHCO3 / aq. ethanol / 2 h / Heating
2: 55 percent / FeSO4*7H2O / aq. NH3 / 1 h / Heating
3: 86 percent / KOH / acetone / 5 h / Heating
4: 70 percent / NH2OH*HCl, pyridine / ethanol / 2 h / Heating
5: 78 percent / aq.NaOH / tetrabutylammonium hydrogen sulphate / 0.5 h / Ambient temperature
View Scheme
参考文献
Shridhar, D. R.; Sastry, C. V. Reddy; Bansal, O. P.; Rao, Pulla; Singh, P. P.; et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 12 p. 1236 - 1242