2H-1,4-苯并噁嗪-3(4H)-酮合成路线 （共 94 条）
反应条件
sodium hydrogencarbonate; N-benzyl-N,N,N-triethylammonium chloride in chloroform 1.) 1 h, 0-5 deg C, 2.) 5 h, 55 deg C;
参考文献
Huang; Chan
Synthesis, 1984 , vol. NO. 10, p. 851 - 852
反应条件
iron; acetic acid T=0°C; 7 h; Inert atmosphereReflux;
参考文献
Rajitha, Chittipaka; Dubey; Sunku, Venkataiah; Veeramaneni, Venugopal Rao; Pal, Manojit
Journal of Heterocyclic Chemistry, 2013 , vol. 50, # 3 p. 630 - 637
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; [C8mim][BF4] T=20°C; 1 h; chemoselective reaction;
参考文献
Sharifi, Ali; Barazandeh, Mehdi; Saeed Abaee; Mirzaei, Mojtaba
Tetrahedron Letters, 2010 , vol. 51, # 14 p. 1852 - 1855
反应条件
iron; acetic acid 2.5 h; Inert atmosphereReflux;
参考文献
Ramesh, Chintakunta; Raju, B. Rama; Kavala, Veerababurao; Kuo, Chun-Wei; Yao, Ching-Fa
Tetrahedron, 2011 , vol. 67, # 6 p. 1187 - 1192
反应条件
hydrogen; palladium on carbon in ethanol T=20°C; 26 h;
参考文献
WO2010/139481 A1, ;
Page/Page column 70 ;
WO 2010/139481 A1
反应条件
samarium; titanium tetrachloride in tetrahydrofuran T=20°C; reductive cyclization; 0.166667 h;
参考文献
Ma; Zhang
Journal of Chemical Research - Part S, 2000 , # 8 p. 388 - 389
反应条件
potassium carbonate in ethyl acetate T=20°C; 10 h;
参考文献
Borate, Hanumant B.; Maujan, Suleman R.; Sawargave, Sangmeshwer P.; Chandavarkar, Mohan A.; Vaiude, Sharangi R.; Joshi, Vinay A.; Wakharkar, Radhika D.; Iyer, Ramki; Kelkar, Ramesh G.; Chavan, Subhash P.; Kunte, Sunita S.
Bioorganic and Medicinal Chemistry Letters, 2010 , vol. 20, # 2 p. 722 - 725
反应条件
copper(l) iodide; 1,10-phenanthroline; caesium carbonate in 1,4-dioxane T=90°C; 24 h; Inert atmosphere;
参考文献
Chen, Dingben; Shen, Guodong; Bao, Weiliang
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 19 p. 4067 - 4073
反应条件
sodium hydrogencarbonate; potassium carbonate in diethyl ether; hexane; chloroform
参考文献
Imperial Chemical Industries PLC; ICI Pharma
Patent: US5217969 A1, 1993 ;
US 5217969 A
反应条件
1.1: aq. KOH / ethanol / 1 h 1.2: 100 percent / dimethylformamide / 24 h 2.1: 70 percent / NaBH4 / Pd/C / dioxane; H2O View Scheme
参考文献
Journal of Agricultural and Food Chemistry, , vol. 54, # 4 p. 991 - 1000
