2-(吡咯烷-1-基)吡啶合成路线 (共 11 条)
反应条件
[Rh(1,5-cyclooctadienyl)(μ-OCH3)]2 in hexane T=80°C; 5 h; Inert atmosphere; regioselective reaction;
参考文献
Kawamorita, Soichiro; Miyazaki, Tatsuya; Iwai, Tomohiro; Ohmiya, Hirohisa; Sawamura, Masaya
Journal of the American Chemical Society, 2012 , vol. 134, # 31 p. 12924 - 12927
反应条件
(IPr)Ni(π-allyl)Cl; sodium t-butanolate in tetrahydrofuran
T=25°C; Buchwald-Hartwig reaction; 3 h; Inert atmosphere;
参考文献
Iglesias, Maria Jose; Prieto, Auxiliadora; Nicasioa, M. Carmen
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 11-12 p. 1949 - 1954
反应条件
potassium phosphate; copper(l) iodide; CVT-2537 in dimethyl sulfoxide
T=90°C; 24 h; Inert atmosphere;
参考文献
Zhang, Yu; Yang, Xinye; Yao, Qizheng; Ma, Dawei
Organic Letters, 2012 , vol. 14, # 12 p. 3056 - 3059
反应条件
sodium carbonate in acetonitrile
T=150°C; 1.5 h; Microwave irradiation;
参考文献
Bergman, Sheba D.; Storr, Thomas E.; Prokopcova, Hana; Aelvoet, Karel; Diels, Gaston; Meerpoel, Lieven; Maes, Bert U. W.
Chemistry - A European Journal, 2012 , vol. 18, # 33 p. 10393 - 10398
反应条件
N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate in dichloromethane
T=25°C; 15 h;
参考文献
Londregan, Allyn T.; Jennings, Sandra; Wei, Liuqing
Organic Letters, 2010 , vol. 12, # 22 p. 5254 - 5257
反应条件
1: in tetrahydrofuran
T=20°C; 1 h;
2: With hydrogenchloride in methanol
12 h; Heating;
参考文献
Thomas, Shannon; Roberts, Sara; Pasumansky, Lubov; Gamsey, Soya; Singaram, Bakthan
Organic Letters, 2003 , vol. 5, # 21 p. 3867 - 3870
反应条件
η5-cyclopentadienyl-η4-cycloocta-1,5-diene-cobalt(I) in toluene
T=25°C; Irradiation;
参考文献
Heller, Barbara; Sundermann, Bernd; Buschmann, Helmut; Drexler, Hans-Joachim; You, Jingsong; Holzgrabe, Ulrike; Heller, Eberhard; Oehme, Guenther
Journal of Organic Chemistry, 2002 , vol. 67, # 13 p. 4414 - 4422
反应条件
dimethylsulfide borane complex in tetrahydrofuran
9 h; Heating;
参考文献
Venuti, Michael C.; Ort, Oswald
Synthesis, 1988 , # 12 p. 985 - 988
反应条件
T=60°C; Substitution; 5 h;
参考文献
D'Andrea, Stan V.; Freeman, Jeremiah P.; Szmuszkovicz, Jacob
Organic Preparations and Procedures International, 1999 , vol. 31, # 6 p. 698 - 701
反应条件
tetrahydrofuran; aluminum oxide
T=390°C;
参考文献
Jur'ew et al.
Zhurnal Obshchei Khimii, 1940 , vol. 10, p. 1839,1840
Chem. Zentralbl., 1942 , vol. 113, # II p. 1458