6-氯-N,N-二甲基-5-硝基-4-嘧啶胺合成路线 (共 2 条)
反应条件
1: 95 percent / methanol / 5 h / Ambient temperature 2: 97 percent / Fe, glacial acetic acid, / methanol / 4 h / Heating 3: 59 percent / sodium nitrite, aq. HCl, / H2O / 1.5 h View Scheme
参考文献
Nemeryuk, Michal P.; Sedov, Andrej L.; Safonova, Tamara S.; Cerny, Antonin; Krepelka, Jiri
Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 1 p. 215 - 233
反应条件
hydrazine hydrate in methanol
T=20°C; 1.33333 h;
参考文献
Guillard, Jerome; Goujon, Fanny; Badol, Perrine; Poullain, Didier
Tetrahedron Letters, 2003 , vol. 44, # 31 p. 5943 - 5945