三丁基(2-噻吩基)锡合成路线 （共 133 条）
反应条件
1: thiophene With n-butyllithium in tetrahydrofuran T=-78°C; 2: tributyltin chloride in tetrahydrofuran T=20°C;
参考文献
Chinese Chemical Letters, , vol. 22, # 7 p. 819 - 822
反应条件
magnesium; ethylene dibromide in tetrahydrofuran T=35°C; Barbier Coupling Reaction; 1 h; SonicationInert atmosphere;
参考文献
Journal of Organometallic Chemistry, , vol. 741-742, # 1 p. 24 - 32
反应条件
n-butyllithium in thiophene; water
参考文献
US5521173 A1, ;
US 5521173 A
反应条件
dichloro bis(acetonitrile) palladium(II) in N,N,N',N',N'',N''-hexamethylphosphoric triamide 20°C, molar ratio distannane/halide 2:1, 80 min;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 33, p. 1044 - 1049
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 5 p. 1137 - 1142
反应条件
dichloro bis(acetonitrile) palladium(II) in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=20°C; 1.33333 h; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 33, p. 1044 - 1049
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 5 p. 1137 - 1142
反应条件
trans-dichloro(1,3-bis-(2,6-diisopentylphenyl)imidazolylidinium)(3-chloro-pyridine); cesium fluoride in 1,4-dioxane T=20 - 80°C; Stille-Migita cross-coupling; 24 h; Molecular sieveInert atmosphere;
参考文献
Dowlut, Meenakshi; Mallik, Debasis; Organ, Michael G.
Chemistry - A European Journal, 2010 , vol. 16, # 14 p. 4279 - 4283
反应条件
copper(l) iodide; cesium fluoride; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=60°C; 8 h;
参考文献
Kobayashi, Kei; Mohamed Ahmed, Mohamed S.; Mori, Atsunori
Tetrahedron, 2006 , vol. 62, # 41 p. 9548 - 9553
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=80 - 90°C; Stille coupling; 24 h;
参考文献
Ismail, Mohamed A.
Journal of Chemical Research, 2006 , # 11 p. 733 - 737
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=60°C; 16 h;
参考文献
Crisp, Geoffrey T.
Synthetic Communications, 1989 , vol. 19, # 1, 2 p. 307 - 316
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=80 - 90°C; Stille coupling; 24 h;
参考文献
Ismail, Mohamed A.
Journal of Chemical Research, 2006 , # 11 p. 733 - 737
