三丁基(2-噻吩基)锡合成路线 （共 133 条）
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
Stille coupling;
参考文献
Kurach, Ewa; Djurado, David; Rimarik, Jan; Kornet, Aleksandra; Wlostowski, Marek; Luke, Vladimir; Pecaut, Jacques; Zagorska, Malgorzata; Pron, Adam
Physical Chemistry Chemical Physics, 2011 , vol. 13, # 7 p. 2690 - 2700
反应条件
tetrakis(triphenylphosphine) palladium(0) in xylene
T=140°C; 1 h;
参考文献
Tanaka, Akira; Terasawa, Takeshi; Hagihara, Hiroyuki; Sakuma, Yuri; Ishibe, Noriko; Sawada, Masae; Takasugi, Hisashi; Tanaka, Hirokazu
Journal of Medicinal Chemistry, 1998 , vol. 41, # 13 p. 2390 - 2410
反应条件
1: With bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide
T=70°C; Stille Coupling; 3 h;
2: With potassium fluoride in methanol; N,N-dimethyl-formamide
T=20°C; 4 h;
参考文献
Bristol-Myers Squibb Company
Patent: US2008/107624 A1, 2008 ;
Location in patent: Page/Page column 64 ;
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
T=90°C; Stille coupling; 24 h;
参考文献
Aldred, Matthew P.; Vlachos, Panos; Contoret, Adam E. A.; Farrar, Simon R.; Chung-Tsoi; Mansoor, Bassam; Woon, Kai L.; Hudson, Robert; Kelly, Stephen M.; O'Neill, Mary
Journal of Materials Chemistry, 2005 , vol. 15, # 31 p. 3208 - 3213
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tris-(o-tolyl)phosphine in tetrahydrofuran
T=80°C; Stille Coupling; 24 h; Inert atmosphereSealed tube;
参考文献
OCEAN'S KING LIGHTING SCIENCE and TECHNOLOGY CO., LT D,
Patent: US2012/302763 A1, 2012 ;
Location in patent: Page/Page column 6 ;
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
Stille coupling; 24 h; Reflux;
参考文献
Kumar, Natarajan Senthil; Mohanakrishnan, Arasambattu K.
Tetrahedron, 2010 , vol. 66, # 30 p. 5660 - 5670
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; cesium fluoride in 1-methyl-pyrrolidin-2-one; hexane
T=20°C; Stille cross-coupling; 6 h;
参考文献
Littke, Adam F.; Schwarz, Lothar; Fu, Gregory C.
Journal of the American Chemical Society, 2002 , vol. 124, # 22 p. 6343 - 6348
反应条件
copper(l) iodide in N,N-dimethyl-formamide
6 h; Ambient temperature;
参考文献
Kang, Suk-Ku; Kim, Won-Yeob; Jiao, Xianghua
Synthesis, 1998 , # 9 p. 1252 - 1254
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
Stille reaction; 20 h; Heating;
参考文献
Nicolas, Yohann; Blanchard, Philippe; Levillain, Eric; Allain, Magali; Mercier, Nicolas; Roncali, Jean
Organic Letters, 2004 , vol. 6, # 2 p. 273 - 276
反应条件
cesium fluoride; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane
T=100°C; Stille coupling; 36 h;
参考文献
Thomas III, Samuel W.; Venkatesan, Koushik; Mueller, Peter; Swager, Timothy M.
Journal of the American Chemical Society, 2006 , vol. 128, # 51 p. 16641 - 16648
