三丁基(2-噻吩基)锡合成路线 （共 133 条）
反应条件
cesium fluoride; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane
T=100°C; Stille coupling; 36 h;
参考文献
Thomas III, Samuel W.; Venkatesan, Koushik; Mueller, Peter; Swager, Timothy M.
Journal of the American Chemical Society, 2006 , vol. 128, # 51 p. 16641 - 16648
反应条件
copper(l) iodide; tri-tert-butyl phosphine; cesium fluoride; palladium dichloride in N,N-dimethyl-formamide
T=45°C; Stille reaction; 15 h;
参考文献
Mee, Simon P. H.; Lee, Victor; Baldwin, Jack E.
Chemistry - A European Journal, 2005 , vol. 11, # 11 p. 3294 - 3308
反应条件
tetrakis(triphenylphosphine) palladium(0); Cu(I) 3-methylsalicylate in tetrahydrofuran
T=50°C; 42 h;
参考文献
Egi, Masahiro; Liebeskind, Lanny S
Organic letters, 2003 , vol. 5, # 6 p. 801 - 802
反应条件
trans-dichloro(1,3-bis-(2,6-diisopentylphenyl)imidazolylidinium)(3-chloro-pyridine); cesium fluoride in 1,4-dioxane
T=20 - 80°C; Stille-Migita cross-coupling; 24 h; Molecular sieveInert atmosphere;
参考文献
Dowlut, Meenakshi; Mallik, Debasis; Organ, Michael G.
Chemistry - A European Journal, 2010 , vol. 16, # 14 p. 4279 - 4283
反应条件
bis-triphenylphosphine-palladium(II) chloride; lithium chloride in tetrahydrofuran
Stille coupling; 24 h; Reflux;
参考文献
Verbeeck, Stefan; Meyers, Caroline; Franck, Philippe; Jutand, Anny; Maes, Bert U. W.
Chemistry - A European Journal, 2010 , vol. 16, # 43 p. 12831 - 12837
反应条件
1,4-diaza-bicyclo[2.2.2]octane; tetrabutyl ammonium fluoride; palladium diacetate in 1,4-dioxane
T=100°C; Stille reaction; 16 h;
参考文献
Li, Jin-Heng; Liang, Yun; Wang, De-Ping; Liu, Wen-Jie; Xie, Ye-Xiang; Yin, Du-Lin
Journal of Organic Chemistry, 2005 , vol. 70, # 7 p. 2832 - 2834
反应条件
tetrakis (triphenylphosphine) palladium (0) in toluene
参考文献
The United States of America as represented by the Secretary of the Air Force
Patent: US6130339 A1, 2000 ;
反应条件
potassium fluoride; 1,4-dicyclohexyl-diazabutadiene; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane
T=100°C; Stille cross-coupling reaction; 16 h;
参考文献
Li, Jin-Heng; Liang, Yun; Xie, Ye-Xiang
Tetrahedron, 2005 , vol. 61, # 30 p. 7289 - 7293
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane
T=100 - 110°C; Stille coupling; 24 h;
参考文献
Ismail, Mohamed A.; Brun, Reto; Easterbrook, Judy D.; Tanious, Farial A.; Wilson, W. David; Boykin, David W.
Journal of Medicinal Chemistry, 2003 , vol. 46, # 22 p. 4761 - 4769
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide
Stille coupling;
参考文献
SmithKline Beecham Corporation
Patent: US6884801 B1, 2005 ;
Location in patent: Page/Page column 28-29 ;
