三丁基(2-噻吩基)锡合成路线 (共 133 条)
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane
T=100°C; Suzuki Coupling; 16 h;
参考文献
VASTOX PLC
Patent: WO2007/91106 A2, 2007 ;
Location in patent: Page/Page column 136 ;
反应条件
bis[di(tert-butyl)chlorophosphine]palladium dichloride in acetonitrile
T=82°C; Stille cross-coupling; 20 h;
参考文献
Lerebours, Rachel; Camacho-Soto, Alexandra; Wolf, Christian
Journal of Organic Chemistry, 2005 , vol. 70, # 21 p. 8601 - 8604
反应条件
copper(l) chloride in N,N-dimethyl-formamide
T=90°C; Substitution; 1 h;
参考文献
Nudelman, Norma S.; Carro, Cecilia
Synlett, 1999 , # 12 p. 1942 - 1944