三丁基(2-噻吩基)锡合成路线 (共 133 条)
参考文献
Powell, Paul; Sosabowski, Michael H.
Journal of Chemical Research, Miniprint, 1995 , # 10 p. 2422 - 2434
反应条件
PhCH2Pd(PPh3)2Cl in toluene 14 h; Heating;
参考文献
Sosabowski, Michael H.; Powell, Paul
Journal of Chemical Research, Miniprint, 1997 , # 1 p. 201 - 219
反应条件
bis-triphenylphosphine-palladium(II) chloride; lithium chloride in tetrahydrofuran Stille coupling; 8 h; Reflux; Kinetics; ConcentrationReagent/catalystTime;
参考文献
Verbeeck, Stefan; Meyers, Caroline; Franck, Philippe; Jutand, Anny; Maes, Bert U. W.
Chemistry - A European Journal, 2010 , vol. 16, # 43 p. 12831 - 12837
反应条件
bis-triphenylphosphine-palladium(II) chloride; lithium chloride in tetrahydrofuran Stille coupling; 24 h; Reflux; Kinetics; ConcentrationReagent/catalystTime;
参考文献
Verbeeck, Stefan; Meyers, Caroline; Franck, Philippe; Jutand, Anny; Maes, Bert U. W.
Chemistry - A European Journal, 2010 , vol. 16, # 43 p. 12831 - 12837
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane Stille coupling; 5 h; Heating;
参考文献
Torun, Lokman; Liu, Shanghao; Madras, Bertha K.; Meltzer, Peter C.
Tetrahedron Letters, 2006 , vol. 47, # 4 p. 599 - 603
反应条件
caesium carbonate; palladium dichloride in acetonitrile T=20°C; Substitution; 3 h;
参考文献
Kang, Suk-Ku; Lee, Sang-Woo; Ryu, Hyung-Chul
Chemical Communications, 1999 , # 20 p. 2117 - 2118
反应条件
water; palladium dichloride in ethylene glycol dimethyl ether 0.333333 h; Ambient temperature;
参考文献
Kang, Suk-Ku; Ho, Pil-Su; Yoon, Seok-Keun; Lee, Ju-Cheol; Lee, Kyung-Ju
Synthesis, 1998 , # 6 p. 823 - 825
反应条件
cesium fluoride in water; N,N-dimethyl-formamide T=40°C; Stille coupling; 8 h;
参考文献
Wu, Lei; Li, Zhi-Wei; Zhang, Feng; He, Yan-Mei; Fan, Qing-Hua
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 6 p. 846 - 862
反应条件
Pd(OAc)2/XPhos; cesium fluoride in ethylene glycol dimethyl ether T=80°C; Stille coupling; 4 h; Inert atmosphere;
参考文献
Naber, John R.; Buchwald, Stephen L.
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 7-8 p. 957 - 961
反应条件
palladium diacetate; copper dichloride in tetrahydrofuran T=23°C; 0.416667 h;
参考文献
Parrish, Jay P.; Flanders, Vincent L.; Floyd, Ryan J.; Jung, Kyung Woon
Tetrahedron Letters, 2001 , vol. 42, # 44 p. 7729 - 7731