三丁基(2-噻吩基)锡合成路线 (共 133 条)
反应条件
caesium carbonate; palladium dichloride in acetonitrile T=20°C; Substitution; 3 h;
参考文献
Kang, Suk-Ku; Lee, Sang-Woo; Ryu, Hyung-Chul
Chemical Communications, 1999 , # 20 p. 2117 - 2118
反应条件
tris(dibenzylideneacetone)dipalladium (0); P(N(CH2Ph)CH2CH2)3N; cesium fluoride in 1,4-dioxane T=110°C; Stille cross-coupling; 48 h;
参考文献
Su, Weiping; Urgaonkar, Sameer; McLaughlin, Patrick A.; Verkade, John G.
Journal of the American Chemical Society, 2004 , vol. 126, # 50 p. 16433 - 16439
反应条件
bis(acetylacetonate)nickel(II) in 1-methyl-pyrrolidin-2-one T=70°C; Arylation; cross-coupling; 8 h;
参考文献
Kang, Suk-Ku; Ryu, Hyung-Chul; Lee, Sang-Woo
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 19 p. 2661 - 2663
反应条件
palladium dichloride in acetonitrile T=20°C; 3 h;
参考文献
Kang; Ryu; Lee
Synthetic Communications, 2001 , vol. 31, # 7 p. 1027 - 1034
反应条件
bis(acetylacetonate)nickel(II) in 1-methyl-pyrrolidin-2-one T=70°C; Arylation; cross-coupling; 8 h;
参考文献
Kang, Suk-Ku; Ryu, Hyung-Chul; Lee, Sang-Woo
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 19 p. 2661 - 2663
反应条件
bis(acetylacetonate)nickel(II) in 1-methyl-pyrrolidin-2-one T=70°C; Arylation; cross-coupling; 8 h;
参考文献
Kang, Suk-Ku; Ryu, Hyung-Chul; Lee, Sang-Woo
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 19 p. 2661 - 2663
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=110°C; 24 h;
参考文献
Hamad Elgazwy, Abdel-Sattar S.
Phosphorus, Sulfur and Silicon and Related Elements, 2000 , vol. 164, p. 131 - 143
反应条件
1-methyl-pyrrolidin-2-one; manganese bromide tetrahydrate; potassium fluoride; para-iodoanisole T=100°C; 8 h; other reagents: p-iodoanisole/CuI/KF, p-iodoanisole/CuI/CsF, p-iodoanisole/MnBr2/LiCl, p-iodoanisole/MnBr2/CsF, iodobenzene/CuI/NaCl;
参考文献
Kang, Suk-Ku; Kim, Jae-Sun; Choi, Sang-Chul
Journal of Organic Chemistry, 1997 , vol. 62, # 13 p. 4208 - 4209
反应条件
1-methyl-pyrrolidin-2-one; potassium fluoride; copper(l) iodide T=90°C; 7 h; other organostannanes, other organic iodides, other reagents: CuI/NaCl, CuI/KCl, CuI/LiCl, CuI/CsF, MnBr2/NaCl, MnBr2/KCl, MnBr2/KF, MnBr2/LiCl, MnBr2/CsF, MnCl2*4H2O, MnI2, DMF presence, other temperature and time; Product distributionMechanism;
参考文献
Kang, Suk-Ku; Kim, Jae-Sun; Choi, Sang-Chul
Journal of Organic Chemistry, 1997 , vol. 62, # 13 p. 4208 - 4209
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene Stille Cross Coupling; 20 h; Inert atmosphere;
参考文献
Xiao, Zuo; Ye, Gang; Liu, Ying; Chen, Shan; Peng, Qian; Zuo, Qiqun; Ding, Liming
Angewandte Chemie - International Edition, 2012 , vol. 51, # 36 p. 9038 - 9041