三丁基(2-噻吩基)锡合成路线 （共 133 条）
反应条件
lithium hydroxide; caesium carbonate; potassium iodide; Merrifield resin; tetrakis(triphenylphosphine) palladium(0) 1.) DMF, 80 deg C, 16 h; 2.) DMF, 60 degC, 24 h; 3.) THF, MeOH, H2O, reflux, 18 h; Yield given. Multistep reaction;
参考文献
Chamoin, Sylvie; Houldsworth, Stephen; Snieckus, Victor
Tetrahedron Letters, 1998 , vol. 39, # 24 p. 4175 - 4178
反应条件
lithium hydroxide; caesium carbonate; potassium iodide; Merrifield resin; tetrakis(triphenylphosphine) palladium(0) 1.) DMF, 80 deg C, 16 h; 2.) DMF, 60 degC, 24 h; 3.) THF, MeOH, H2O, reflux, 18 h; Yield given. Multistep reaction;
参考文献
Chamoin, Sylvie; Houldsworth, Stephen; Snieckus, Victor
Tetrahedron Letters, 1998 , vol. 39, # 24 p. 4175 - 4178
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran Heating;
参考文献
Bailey, Thomas R.
Tetrahedron Letters, 1986 , vol. 27, # 37 p. 4407 - 4410
反应条件
PhCH2Pd(PPh3)2Cl in toluene 11 h; Heating;
参考文献
Powell, Paul; Sosabowski, Michael H.
Journal of Chemical Research, Miniprint, 1995 , # 10 p. 2422 - 2434
反应条件
1-methyl-pyrrolidin-2-one; copper(l) iodide; sodium chloride T=100°C; 12 h; other reagents: MnBr2/NaCl/N-methylpyrrolidone, MnBr2/NaCl/DMF;
参考文献
Journal of Organic Chemistry, , vol. 62, # 13 p. 4208 - 4209
反应条件
palladium dichloride in water; acetonitrile 0.5 h; Ambient temperature;
参考文献
Synthetic Communications, , vol. 26, # 23 p. 4311 - 4318
反应条件
palladium dichloride in acetonitrile T=20°C; Arylation; 3 h;
参考文献
Journal of Organometallic Chemistry, , vol. 610, # 1-2 p. 38 - 41
反应条件
triphenylphosphine in tetrahydrofuran; N,N-dimethyl-formamide T=80°C; 18 h;
参考文献
European Journal of Organic Chemistry, , # 24 p. 4019 - 4031
反应条件
palladium dichloride in acetonitrile T=20°C; 3 h;
参考文献
Synthetic Communications, , vol. 31, # 7 p. 1027 - 1034
反应条件
palladium dichloride in acetonitrile T=20°C; 3 h;
参考文献
Synthetic Communications, , vol. 31, # 7 p. 1027 - 1034
