三丁基(2-噻吩基)锡合成路线 （共 133 条）
反应条件
palladium dichloride in acetonitrile T=20°C; Arylation;
参考文献
Journal of Organometallic Chemistry, , vol. 610, # 1-2 p. 38 - 41
反应条件
palladium dichloride in water; acetonitrile 0.25 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 37, # 21 p. 3723 - 3726
反应条件
palladium dichloride in water; acetonitrile 0.333333 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 37, # 21 p. 3723 - 3726
反应条件
lithium hydroxide; caesium carbonate; potassium iodide; Merrifield resin; tetrakis(triphenylphosphine) palladium(0) 1.) DMF, 80 deg C, 16 h; 2.) DMF, 60 degC, 24 h; 3.) THF, MeOH, H2O, reflux, 18 h; Yield given. Multistep reaction;
参考文献
Chamoin, Sylvie; Houldsworth, Stephen; Snieckus, Victor
Tetrahedron Letters, 1998 , vol. 39, # 24 p. 4175 - 4178
反应条件
potassium carbonate; tris-(o-tolyl)phosphine; copper(l) chloride; tris-(dibenzylideneacetone)dipalladium(0) in N,N-dimethyl-formamide T=60°C; 0.0833333 h;
参考文献
Suzuki, Masaaki; Doi, Hisashi; Bjoerkman, Margareta; Andersson, Yvonne; Langstroem, Bengt; Watanabe, Yasuyoshi; Noyori, Ryoji
Chemistry - A European Journal, 1997 , vol. 3, # 12 p. 2039 - 2042
反应条件
tetrakis(triphenylphosphine) palladium(0) 1.) reflux, 2 h, 2.) reflux, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Sandosham, Jessie; Undheim, Kjell; Rise, Frode
Heterocycles, 1993 , vol. 35, # 1 p. 235 - 244
反应条件
bis[di(tert-butyl)chlorophosphine]palladium dichloride in acetonitrile T=82°C; Stille cross-coupling; 20 h;
参考文献
Lerebours, Rachel; Camacho-Soto, Alexandra; Wolf, Christian
Journal of Organic Chemistry, 2005 , vol. 70, # 21 p. 8601 - 8604
反应条件
palladium dichloride in water; acetonitrile 0.333333 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 37, # 21 p. 3723 - 3726
反应条件
water; palladium dichloride in ethylene glycol dimethyl ether 0.333333 h; Ambient temperature;
参考文献
Kang, Suk-Ku; Ho, Pil-Su; Yoon, Seok-Keun; Lee, Ju-Cheol; Lee, Kyung-Ju
Synthesis, 1998 , # 6 p. 823 - 825
反应条件
mercury(II) trifluoroacetate in chloroform; acetic acid stirring the mixt. in dry CHCl3 in a stoppered flask (30 min), addn. of CH3COOH, stirring (5 min); evapn., dissolving residue in a min. vol. of CHCl3-CH3COOH (19:1), slowly pouring the soln. into dry light petroleum, pptn., filtration at the pump under a stream of dry N2, drying in vac.;
参考文献
Pinhey, John T.; Roche, Eric G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2415 - 2422
