三丁基(2-噻吩基)锡合成路线 (共 133 条)
反应条件
palladium(II) dichloride bis[bis(diphenylphosphine)ferrocene] dichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl-formamide T=100°C; Stille coupling; 16 h;
参考文献
Saevmarker, Jonas; Lindh, Jonas; Nilsson, Peter
Tetrahedron Letters, 2010 , vol. 51, # 52 p. 6886 - 6889
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=90°C; 45 h;
参考文献
Gundersen, Lise-Lotte
Tetrahedron Letters, 1994 , vol. 35, # 19 p. 3155 - 3158
反应条件
palladium diacetate in tetrahydrofuran T=20°C; Stille reaction; 1.5 h;
参考文献
Dughera, Stefano
Synthesis, 2006 , # 7 p. 1117 - 1122
反应条件
palladium diacetate; cesium fluoride; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tert-butyl alcohol T=110°C; Stille coupling; 14 h; Inert atmosphere;
参考文献
Naber, John R.; Fors, Brett P.; Wu, Xiaoxing; Gunn, Jonathon T.; Buchwald, Stephen L.
Heterocycles, 2010 , vol. 80, # 2 p. 1215 - 1226
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane 8 h; Heating;
参考文献
Brendle, James J.; Outlaw, Abram; Kumar, Arvind; Boykin, David W.; Patrick, Donald A.; Tidwell, Richard R.; Werbovetz, Karl A.
Antimicrobial Agents and Chemotherapy, 2002 , vol. 46, # 3 p. 797 - 807
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene 12 h; Inert atmosphereReflux;
参考文献
Sumitomo Chemical Company, Limited; Osaka University
Patent: EP2407464 A1, 2012 ;
Location in patent: Page/Page column 24 ;
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=60°C; 16 h;
参考文献
Crisp, Geoffrey T.
Synthetic Communications, 1989 , vol. 19, # 1, 2 p. 307 - 316
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene Stille coupling; RefluxInert atmosphere;
参考文献
Leriche, Philippe; Aillerie, David; Roquet, Sophie; Allain, Magali; Cravino, Antonio; Frere, Pierre; Roncali, Jean
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 17 p. 3202 - 3207
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene Stille coupling; 12 h; RefluxInert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 6, # 17 p. 3202 - 3207
反应条件
tris-(dibenzylideneacetone)dipalladium(0); triphenyl-arsane in toluene Stille Cross Coupling; 20 h; Inert atmosphereReflux;
参考文献
Scrascia, Angela; De Marco, Luisa; Laricchia, Savio; Picca, Rosaria Anna; Carlucci, Claudia; Fabiano, Eduardo; Capodilupo, Agostina Lina; Della Sala, Fabio; Gigli, Giuseppe; Ciccarella, Giuseppe
Journal of Materials Chemistry A, 2013 , vol. 1, # 38 p. 11909 - 11921