三丁基(2-噻吩基)锡合成路线 （共 133 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine in tetrahydrofuran T=60°C; decarbonylative Stille coupling; 1 h; Inert atmosphere;
参考文献
Tasch, Boris O. A.; Merkul, Eugen; Frank, Walter; Mueller, Thomas J.J.
Synthesis, 2010 , # 13 art. no. C01410SS, p. 2139 - 2146
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=60°C; 16 h;
参考文献
Crisp, Geoffrey T.
Synthetic Communications, 1989 , vol. 19, # 1, 2 p. 307 - 316
反应条件
tetrakis(triphenylphosphine) palladium(0); Cu(I) 3-methylsalicylate in tetrahydrofuran T=50°C; 14 h;
参考文献
Egi, Masahiro; Liebeskind, Lanny S
Organic letters, 2003 , vol. 5, # 6 p. 801 - 802
反应条件
bis-triphenylphosphine-palladium(II) chloride; lithium chloride in 1,4-dioxane T=90°C; 16 h;
参考文献
Crisp, Geoffrey T.; Papadopoulos, Spiros
Australian Journal of Chemistry, 1989 , vol. 42, # 2 p. 279 - 285
反应条件
1: With tetrakis(triphenylphosphine) palladium(0) in xylene 4 h; Heating / reflux; 2: With potassium fluoride in water; toluene; xylene T=20°C; 2 h;
参考文献
Merck and Co., Inc.
Patent: US6642237 B1, 2003 ;
Location in patent: Page/Page column 183 ;
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=55 - 105°C; Stille cross-coupling;
参考文献
Destri, Silvia; Pasini, Mariacecilia; Botta, Chiara; Porzio, William; Bertini, Fabio; Marchio, Luciano
Journal of Materials Chemistry, 2002 , vol. 12, # 4 p. 924 - 933
反应条件
sulfuryl dichloride in tetrachloromethane 6 h;
参考文献
Lube, Andreas; Neumann, Wilhelm P.; Niestroj, Michael
Chemische Berichte, 1995 , vol. 128, # 12 p. 1195 - 1198
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=80°C;
参考文献
Gohier, Frederic; Frere, Pierre; Roncali, Jean
Journal of Organic Chemistry, 2013 , vol. 78, # 4 p. 1497 - 1503
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene Inert atmosphere;
参考文献
Porzio, William; Destri, Silvia; Pasini, Mariacecilia; Giovanella, Umberto; Ragazzi, Massimo; Scavia, Guido; Kotowski, Dariusz; Zotti, Gianni; Vercelli, Barbara
New Journal of Chemistry, 2010 , vol. 34, # 9 p. 1961 - 1973
反应条件
trans-dichloro(1,3-bis-(2,6-diisopentylphenyl)imidazolylidinium)(3-chloro-pyridine); cesium fluoride in 1,4-dioxane T=20 - 60°C; Stille-Migita cross-coupling; 24 h; Molecular sieveInert atmosphere;
参考文献
Dowlut, Meenakshi; Mallik, Debasis; Organ, Michael G.
Chemistry - A European Journal, 2010 , vol. 16, # 14 p. 4279 - 4283
