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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5467-84-5
合成路线
（共 26 条）
7647-01-0
盐酸
+
5467-84-5
→
反应条件
64-04-0
2-苯乙胺
反应条件
T=180°C;
参考文献
Thiele; Pickard
Justus Liebigs Annalen der Chemie, 1899 , vol. 309, p. 193
1943-82-4
2-苯乙基异氰酸酯
→
反应条件
5467-84-5
反应条件
[Pr(SPh)3(THF)3] in tetrahydrofuran T=60°C; 12 h; Inert atmosphere;
参考文献
Wang, He-Ming; Li, Hong-Xi; Yu, Xiang-Yang; Ren, Zhi-Gang; Lang, Jian-Ping
Tetrahedron, 2011 , vol. 67, # 8 p. 1530 - 1535
201230-82-2
+
64-04-0
2-苯乙胺
→
反应条件
5467-84-5
反应条件
copper diacetate; air; palladium diacetate in toluene P=760 Torr; 2 h; Heating;
参考文献
Orito, Kazuhiko; Miyazawa, Mamoru; Nakamura, Takatoshi; Horibata, Akiyoshi; Ushito, Harumi; Nagasaki, Hideo; Yuguchi, Motoki; Yamashita, Satoshi; Yamazaki, Tetsuro; Tokuda, Masao
Journal of Organic Chemistry, 2006 , vol. 71, # 16 p. 5951 - 5958
124-38-9
二氧化碳
+
64-04-0
2-苯乙胺
→
反应条件
5467-84-5
反应条件
1: phenethylamine With titanium tetrachloride in dichloromethane T=0°C; 0.5 h; Inert atmosphere; 2: With pyridine in dichloromethane 0.5 h; Inert atmosphere; 3: carbon dioxide Further stages;
参考文献
Anderson, James C.; Moreno, Rafael Bou
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 7 p. 1334 - 1338
64-04-0
2-苯乙胺
→
反应条件
5467-84-5
反应条件
tributylphosphine; 2-methyl-but-3-yn-2-ol; ruthenium trichloride T=140°C; P=37503 Torr; 20 h;
参考文献
Fournier, Jean; Bruneau, Christian; Dixneuf, Pierre H.; Lecolier, Serge
Journal of Organic Chemistry, 1991 , vol. 56, # 14 p. 4456 - 4458
64-04-0
2-苯乙胺
+
57-13-6
尿素
→
反应条件
5467-84-5
反应条件
1,2,3-Benzotriazole in neat (no solvent) T=120°C; 24 h; Inert atmosphere;
参考文献
Nguyen, Thanh Binh; Ermolenko, Ludmila; Dau, Marie-Elise Tran Huu; Al-Mourabit, Ali
Heterocycles, 2014 , vol. 88, # 1 p. 403 - 416
1124-32-9
→
反应条件
5467-84-5
+
66773-34-0
反应条件
copper(ll) bromide in tetrahydrofuran T=20°C; 3.25 h;
参考文献
Yamaguchi, Jun-Ichi; Murayama, Yukihito; Suyama, Takayuki
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 2 p. 329 - 333
1202680-24-7
+
64-04-0
2-苯乙胺
→
反应条件
5467-84-5
反应条件
1: in tetrahydrofuran T=20°C; 2: With 4-(N,N-dimethlyamino)pyridine in tetrahydrofuran Reflux;
参考文献
Lee, Hyung-Geun; Kim, Min-Jung; Park, Song-Eun; Kim, Jeum-Jong; Kim, Bo Ram; Lee, Sang-Gyeong; Yoon, Yong-Jin
Synlett, 2009 , # 17 p. 2809 - 2814
102-01-2
N-乙酰乙酰苯胺
+
64-04-0
2-苯乙胺
→
反应条件
5467-84-5
反应条件
zeolite HSZ-360 T=180°C; Condensation; 3 h;
参考文献
Bigi, Franca; Frullanti, Bettina; Maggi, Raimondo; Sartori, Giovanni; Zambonin, Elena
Journal of Organic Chemistry, 1999 , vol. 64, # 3 p. 1004 - 1006
→
反应条件
5467-84-5
反应条件
1: [Ti(NtBu)Cl2py3]; phenethylamine in dichloromethane T=20 - 25°C; 2 h; Inert atmosphere; 2: carbon dioxide in dichloromethane T=20 - 25°C; P=1140.08 Torr; 5 h; Inert atmosphere; 3: With hydrogenchloride in dichloromethane; water 1 h;
参考文献
Anderson, James C.; Moreno, Rafael Bou
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 7 p. 1334 - 1338
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