苯乙醛 1,3-丙烷二基缩醛合成路线 (共 4 条)
反应条件
in water; N,N-dimethyl-formamide
参考文献
Astra Pharmaceuticals Limited
Patent: US5648370 A1, 1997 ;
US 5648370 A
反应条件
iodine in 1,4-dioxane; chloroform
24 h; Reflux;
参考文献
Kumar, Macharla Arun; Swamy, Peraka; Naresh, Mameda; Reddy, Marri Mahender; Rohitha, Chozhiyath Nappunni; Prabhakar, Sripadi; Sarma, Akella Venkata Subrahmanya; Kumar, Joseph Richard Prem; Narender, Nama
Chemical Communications, 2013 , vol. 49, # 17 p. 1711 - 1713
反应条件
disodium hydrogenphosphate; oxygen; dichloro bis(acetonitrile) palladium(II); copper(l) chloride in ethylene glycol dimethyl ether
T=65°C; P=760 Torr; 48 h; Yield given. Yields of byproduct given;
参考文献
Hosokawa; Ataka; Murahashi
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 1 p. 166 - 169
反应条件
toluene-4-sulfonic acid in benzene
10 h; Heating;
参考文献
Suginome, Hiroshi; Wang, Jian Bo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 10 p. 2825 - 2829