(±)-3-羟基-r-丁内酯合成路线 （共 44 条）
反应条件
sodium hydroxide; Enterobacter sp.DS-S-75 T=30°C; pH=6.7; 40 h; Enzymatic reaction; Product distribution; Further Variations:Reagents;
参考文献
Advanced Synthesis and Catalysis, , vol. 345, # 4 p. 437 - 455
反应条件
camphor-10-sulfonic acid; tetrabutyl ammonium fluoride Yield given. Multistep reaction;
参考文献
Heterocycles, , vol. 30, # 2 p. 745 - 748
反应条件
β-glucosidase in water T=37°C; 5 h; Product distribution;
参考文献
Biological and Pharmaceutical Bulletin, , vol. 23, # 6 p. 731 - 734
反应条件
hydrogenchloride; sodium hydroxide 1.) reflux, 1 h, 2.) reflux, 3 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Liebigs Annales, , # 9 p. 1877 - 1879
反应条件
Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 21 p. 2855 - 2862
参考文献
Angewandte Chemie, , vol. 101, # 4 p. 484 - 485
反应条件
sodium borohydride in ethanol
参考文献
Daiso Co., Ltd.
Patent: US6949684 B2, 2005 ;
Title/Abstract Full Text Show Details
Ikai, Kousei; Mikami, Masafumi; Furukawa, Yoshiro; Urano, Takeshi; Ohtaka, Seiji
Patent: US2003/45759 A1, 2003 ;
反应条件
sodium borohydride in ethanol
参考文献
Daiso Co., Ltd.
Patent: US6949684 B2, 2005 ;
Title/Abstract Full Text Show Details
Ikai, Kousei; Mikami, Masafumi; Furukawa, Yoshiro; Urano, Takeshi; Ohtaka, Seiji
Patent: US2003/45759 A1, 2003 ;
反应条件
hydrogen bromide; sodium acetate in dichloromethane; acetic acid
参考文献
Samsung Fine Chemicals Co., Ltd.
Patent: US6586616 B1, 2003 ;
反应条件
1,4-dioxane; phosphorus pentoxide
参考文献
Glattfeld; Stack
Journal of the American Chemical Society, 1937 , vol. 59, p. 753,757
