1,3-丙二醇-二-间-甲苯磺酸盐合成路线 （共 22 条）
反应条件
potassium iodide; silver(l) oxide in dichloromethane T=20°C; 1 h;
参考文献
Organic Letters, , vol. 4, # 14 p. 2329 - 2332
反应条件
pyridine T=0°C; 3 h;
参考文献
Yamamoto, Fumihiko; Oka, Hidenobu; Antoku, Shigetoshi; Ichiya, Yu-Ichi; Masuda, Kouji; Maeda, Minoru
Biological and Pharmaceutical Bulletin, 1999 , vol. 22, # 6 p. 590 - 597
反应条件
sodium hydroxide in tetrahydrofuran; water T=0°C;
参考文献
Journal of Organic Chemistry, , vol. 57, # 18 p. 4998 - 5005
反应条件
1: 1-chloro-2-methoxy-ethane; Trimethylene glycol With sodium hydroxide; water Etherification; 25 h; Heating; 2: p-toluenesulfonyl chloride With pyridine Esterification;
参考文献
Tamai, Yasufumi; Hattori, Tetsutaro; Date, Masamitsu; Koike, Shinji; Kamikubo, Yoshinori; Akiyama, Masahiro; Seino, Kazuhiro; Takayama, Hideki; Oyama, Tomohito; Miyano, Sotaro
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 12 p. 1685 - 1694
反应条件
sodium carbonate in acetonitrile 144 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Springborg, Johan; Kofod, Pauli; Olsen, Carl Erik; Toftlund, Hans; Soetofte, Inger
Acta Chemica Scandinavica, 1995 , vol. 49, # 8 p. 547 - 554
反应条件
CuBr*Me2S-LiBr; lithium thiophenoxide; magnesium 1) THF, reflux; 2) THF, HMPA, rt, 24 h; further reagents and conditions; Yield given. Multistep reaction;
参考文献
Burns, Dennis H.; Miller, Jeffrey D.; Chan, Ho-Kit; Delaney, Michael O.
Journal of the American Chemical Society, 1997 , vol. 119, # 9 p. 2125 - 2133
反应条件
sodium iodide in acetone Heating;
参考文献
Lichtenberger,J.; Tritsch,P.
Bulletin de la Societe Chimique de France, 1961 , p. 369 - 371
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in benzene Heating;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 27, # 1-12 p. 790 - 792
反应条件
sodium hydride in various solvents; N,N-dimethyl-formamide T=105°C; 8 h;
参考文献
Gao, Jinzhang; He, Hui; Zhang, Xuan; Lu, Xiaoquan; Kang, Jingwan
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 2 p. 372 - 375
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=80°C; 0.25 h;
参考文献
Zea-Ponce, Yolanda; Mavel, Sylvie; Assaad, Thaer; Kruse, Shane E.; Parsons, Stanley M.; Emond, Patrick; Chalon, Sylvie; Giboureau, Nicolas; Kassiou, Michael; Guilloteau, Denis
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 3 p. 745 - 753
