1,3-丙二醇-二-间-甲苯磺酸盐合成路线 （共 22 条）
反应条件
sodium hydroxide in water
Heating;
参考文献
Lichtenberger,J.; Tritsch,P.
Bulletin de la Societe Chimique de France, 1961 , p. 369 - 371
反应条件
in N,N-dimethyl-formamide
参考文献
Pisareva, S. A.; Bel'skii, F. I.; Medved', T. Ya.; Kabachnik, M. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 2 p. 372 - 376
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 2 p. 413 - 417
反应条件
sodium hydride in N,N-dimethyl-formamide
1.) 30 min, 2.) 120 - 125 deg C, 8 h; Yield given;
参考文献
Subramanian, S.; Bridson, J.; Miller, D.
Journal of Chemical Crystallography, 1995 , vol. 25, # 11 p. 743 - 746
反应条件
sodium hydroxide in water
Heating;
参考文献
Lichtenberger,J.; Tritsch,P.
Bulletin de la Societe Chimique de France, 1961 , p. 369 - 371
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in benzene
Heating;
参考文献
Singh, Paramjit; Jain, Anupa
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, # 1-12 p. 790 - 792
反应条件
in N,N-dimethyl-formamide
参考文献
Houser, Robert P.; Young Jr., Victor G.; Tolman, William B.
Journal of the American Chemical Society, 1996 , vol. 118, # 8 p. 2101 - 2102
反应条件
sodium hydride
1.) DMF, 100 deg C, 30 min, 2.) DMF, 100 deg C; Yield given. Multistep reaction;
参考文献
Ewin, Gavin; Hill, John O.
Journal of Chemical Research, Miniprint, 1985 , # 11 p. 3501 - 3519
反应条件
sodium hydroxide; potassium carbonate in water
T=120°C; P=2068.59 - 4137.18 Torr; 0.333333 h; microwave irradiation;
参考文献
Ju, Yuhong; Varma, Rajender S.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 135 - 141
反应条件
sodium hydride
1) THF, 30 min, r.t., 2) THF, 6 h, reflux; Yield given. Multistep reaction;
参考文献
Weber, Edwin
Chemische Berichte, 1981 , vol. 114, # 4 p. 1551 - 1553
反应条件
dilithium tetrachlorocuprate; magnesium
1.) THF; 2.) THF, 25 deg C, 48 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Burns, Dennis H.; Miller, Jeffrey D.
Tetrahedron Letters, 1994 , vol. 35, # 29 p. 5189 - 5192
