反应条件
1: 1,6-dibromo-2,4-hexadiyne With potassium tert-butylate in tetrahydrofuran T=-78 - -60°C; 2 h; Inert atmosphere; 2: chloro-trimethyl-silane in tetrahydrofuran T=-60°C; 3.5 h; Inert atmosphere;
参考文献
Decicco, Racquel C.; Black, Allison; Li, Lei; Goroff, Nancy S.
European Journal of Organic Chemistry, 2012 , # 25 p. 4699 - 4704