Birman's catalyst; trimethylacetic anhydride; N-ethyl-N,N-diisopropylamine in diethyl ether T=20°C; 12 h; Inert atmosphereResolution of racemate; optical yield given as percent eeenantioselective reaction;
参考文献
Tokyo University of Science Educational Foundation Administrative Organization
Patent: US2011/319650 A1, 2011 ;
Location in patent: Page/Page column 11 ;
immobilized lipase B from Candida antarctica in tert-butyl methyl ether T=65°C; 4 h; Resolution of racemateEnzymatic reaction; Temperature; enantioselective reaction;
参考文献
Lee, Yeon Soo; Hong, Joo Hee; Jeon, Nan Young; Won, Keehoon; Kim, Bum Tae
Organic Process Research and Development, 2004 , vol. 8, # 6 p. 948 - 951
immobilized lipase B from Candida antarctica in tert-butyl methyl ether T=65°C; 3 h; Resolution of racemateEnzymatic reaction; Temperature; enantioselective reaction;
参考文献
Lee, Yeon Soo; Hong, Joo Hee; Jeon, Nan Young; Won, Keehoon; Kim, Bum Tae
Organic Process Research and Development, 2004 , vol. 8, # 6 p. 948 - 951
immobilized lipase B from Candida antarctica in tert-butyl methyl ether T=65°C; 2 h; Resolution of racemateEnzymatic reaction; Temperature; enantioselective reaction;
参考文献
Lee, Yeon Soo; Hong, Joo Hee; Jeon, Nan Young; Won, Keehoon; Kim, Bum Tae
Organic Process Research and Development, 2004 , vol. 8, # 6 p. 948 - 951