phosphate buffer in water
soln. of Na(15)NO2 in H2O and mixt. of NH2OH*HCl with phosphate buffer (pH 7-9) were degassed on the vac. line by successive freeze-pump-thaw cycles, mixed, the reaction was initiated by rotation of the vessel, after 48 h aq. phase was frozen at 194K; collected at 77K;
参考文献
Bonner, Francis T.; Kada, John; Phelan, Kieran G.
Inorganic Chemistry, 1983 , vol. 22, p. 1389 - 1391
in further solvent(s)
react. in tetrachlorethane at 100 °C;;
参考文献
Becke-Goehring, M.; Gehrmann, W.; Goetze, W.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1963 , vol. 326, p. 127 - 138
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Gmelin Handbook: P: MVol.C, 192, page 441 - 443