反应条件
1: cyclopropane carboxylic acid cyanide With gallium trifluoromethanesulfonate; ammonia in dichloromethane
T=-78°C; 3 h; Inert atmosphere;
2: hydrogen cyanide in dichloromethane
T=-78 - 25°C; Inert atmosphere;
3: carbon dioxide With N-ethyl-N,N-diisopropylamine in dichloromethane
T=25°C; 3 h; Inert atmosphere;
参考文献
Murray, Ross G.; Whitehead, David M.; Le Strat, Franck; Conway, Stuart J.
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 6 p. 988 - 991