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Lipase;

1: 90 percent / pyridine / Ambient temperature 2: 77 percent / diethyl ether / 1.) -40 deg C, 3 h, 2.) room temperature, overnight 3: 82 percent / LiAlH4 / diethyl ether / 3 h / Heating View Scheme

1: 90 percent / pyridine / Ambient temperature 2: 77 percent / diethyl ether / 1.) -40 deg C, 3 h, 2.) room temperature, overnight 3: 82 percent / LiAlH4 / diethyl ether / 3 h / Heating 4: 72 percent / PCC / CH2Cl2 / 3 h / Ambient temperature View Scheme

1: 90 percent / pyridine / Ambient temperature 2: 77 percent / diethyl ether / 1.) -40 deg C, 3 h, 2.) room temperature, overnight View Scheme