1,2-二(3,4-二甲氧基苯基)乙胺合成路线 （共 12 条）
反应条件
1: K2CO3 2: phosphorus (V)-oxide; tetralin / 140 - 170 °C 3: aqueous KOH-solution; aqueous potassium permanganate View Scheme
参考文献
Waldmann; Chwala
Justus Liebigs Annalen der Chemie, 1957 , vol. 609, p. 125,141
反应条件
PPA in dichloromethane T=80°C; 3 h;
参考文献
Venkov, Atanas P.; Ivanov, Ilian I.
Tetrahedron, 1996 , vol. 52, # 37 p. 12299 - 12308
反应条件
1: formic acid
2: aqueous H2SO4
View Scheme
参考文献
Battersby; Binks
Journal of the Chemical Society, 1958 , p. 4333,4337
反应条件
potassium hydroxide; diethylene glycol
参考文献
Walker
Journal of the American Chemical Society, 1954 , vol. 76, p. 3999,4001
反应条件
sodium amalgam; ethanol; acetic acid
参考文献
Allen; Buck
Journal of the American Chemical Society, 1930 , vol. 52, p. 310,312
反应条件
1: ueber das Azid
2: KOH; aqueous diethylene glycol
View Scheme
参考文献
Walker
Journal of the American Chemical Society, 1954 , vol. 76, p. 3999,4001
反应条件
1: AlCl3; carbon disulfide
3: sodium-amalgam; ethanol; acetic acid
View Scheme
参考文献
Allen; Buck
Journal of the American Chemical Society, 1930 , vol. 52, p. 310,312
反应条件
1: ethanol; tin; aqueous CuSO4 / Reagens 4:wss.HCl
3: sodium-amalgam; ethanol; acetic acid
View Scheme
参考文献
Allen; Buck
Journal of the American Chemical Society, 1930 , vol. 52, p. 310,312
反应条件
1: AlCl3; carbon disulfide
3: sodium-amalgam; ethanol; acetic acid
View Scheme
参考文献
Allen; Buck
Journal of the American Chemical Society, 1930 , vol. 52, p. 310,312
反应条件
1: LiAlH4 / tetrahydrofuran
2: (i) 3,4-dimethoxy-benzaldehyde, benzene, (ii) NaH, DMF, (iii) /BRN= 973727/
View Scheme
参考文献
Battersby,A.R. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 1162 - 1171
