1,3-二苯基异苯并呋喃合成路线 （共 125 条）
反应条件
carbon disulfide; diphosphorus pentasulfide
参考文献
Dufraisse; Daniel
Bulletin de la Societe Chimique de France, 1937 , vol. <5> 4, p. 2063,2068
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Wittig et al.
Justus Liebigs Annalen der Chemie, 1960 , vol. 630, p. 15
反应条件
potassium tert-butylate in dimethyl sulfoxide
参考文献
Wittig,G.; Fritze,P.
Justus Liebigs Annalen der Chemie, 1968 , vol. 711, p. 82 - 87
反应条件
isopentyl nitrite in toluene T=80 - 100°C; 3 h;
参考文献
CANON KABUSHIKI KAISHA; KAMATANI, Jun; YAMADA, Naoki; KISHINO, Kengo; SAITOH, Akihito
Patent: WO2011/152477 A1, 2011 ;
Location in patent: Page/Page column 36-37 ;
反应条件
in ethanol
T=39.5°C; var. conc. of DPBF; Rate constant;
参考文献
Frandsen; Hakansson; Holm; Harrit
Acta chemica Scandinavica (Copenhagen, Denmark : 1989), 1991 , vol. 45, # 6 p. 627 - 631
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
T=20°C; P=2585.7 Torr; 12 h;
参考文献
Smith, James G.; McCall, Robert B.
Journal of Organic Chemistry, 1980 , vol. 45, # 20 p. 3982 - 3986
反应条件
xylene
lower-melting stereoisomer(ic);
参考文献
Dufraisse; Priou
Bulletin de la Societe Chimique de France, 1938 , vol. <5> 5, p. 502,507
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Weiss; Abeles
Monatshefte fuer Chemie, 1932 , vol. 61, p. 162,165
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Bergmann
Journal of the Chemical Society, 1938 , p. 1147,1150
反应条件
n-butyllithium in tetrahydrofuran; hexane
0.5 h; temperature < -70 deg; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Coates, Robert M.; Last, Larry A.
Journal of the American Chemical Society, 1983 , vol. 105, # 25 p. 7322 - 7326
反应条件
n-butyllithium in tetrahydrofuran; hexane
0.5 h; temperature < -70 deg; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Coates, Robert M.; Last, Larry A.
Journal of the American Chemical Society, 1983 , vol. 105, # 25 p. 7322 - 7326
反应条件
1: Na / tetrahydrofuran / 8 h
2: 82 percent / -70 °C
3: 96 percent / p-Toluenesulfonic acid / benzene / 12 h / Heating
View Scheme
参考文献
Weiss; Abeles
Monatshefte fuer Chemie, 1932 , vol. 61, p. 162,165
参考文献
Paquette,L.A. et al.
Journal of the American Chemical Society, 1978 , vol. 100, # 5 p. 1597 - 1599
