3-甲基-2-硝基苯甲酸甲酯合成路线 （共 18 条）
反应条件
thionyl chloride T=0 - 20°C; 10 h; Inert atmosphere; Reagent/catalystTime;
参考文献
Tetrahedron, , vol. 69, # 32 p. 6679 - 6686
反应条件
sodium hydroxide; thionyl chloride in methanol; water
反应条件
in hexane; acetone 3 h;
参考文献
US2005/222141 A1, ;
Page/Page column 30 ;
参考文献
Journal of the Chemical Society, , p. 2067,2070
反应条件
1: fuming nitric acid 2: HCl View Scheme
参考文献
Chemische Berichte, , vol. 40, p. 4413
参考文献
Chemische Berichte, , vol. 42, p. 433
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 20, p. 162
反应条件
sodium tetrahydroborate in tetrahydrofuran 1.5 h; Heating / reflux;
参考文献
EP1431278 A1, ;
Page 15 ;
反应条件
1: 55 percent / dibenzoyl peroxide, NBS / CCl4 / 23.5 h / 90 °C / Irradiation 2: 75 percent / CHCl3 / 0.25 h / Heating 3: 100 percent / Et3N / CH2Cl2 / 0.08 h / Ambient temperature 4: 71 percent / PPh3, CO / Pd(OAc)2 / acetonitrile / 75 h / 3040 Torr / Heating View Scheme
参考文献
Kamiya; Matsui; Shirahase; Nakamura; Wada; Kanda; Shimaji; Kakeya
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 10 p. 1692 - 1695
