7-(二乙基氨基)-4-(羟基甲基)-2H-苯并吡喃-2-酮合成路线 （共 11 条）
反应条件
sodium tetrahydroborate in isopropyl alcohol
T=20°C; 1 h;
参考文献
Weis, Simone; Shafiq, Zahid; Gropeanu, Radu A.; Del Campo, Aranzazu
Journal of Photochemistry and Photobiology A: Chemistry, 2012 , vol. 241, p. 52 - 57
反应条件
1: in para-xylene
24 h; Heating;
2: With sodium tetrahydroborate in ethanol
T=20°C; 4 h;
参考文献
Schoenleber, Ralph O; Bendig, Juergen; Hagen, Volker; Giese, Bernd
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 1 p. 97 - 101
反应条件
selenium(IV) oxide; sodium borohydride in ethanol; para-xylene
参考文献
Cornell Research Foundation, Inc.
Patent: US2007/243519 A1, 2007 ;
反应条件
1: trifluoroacetic acid / dichloromethane / 2.5 h / 20 °C / Darkness
2: water / Photolysis
View Scheme
参考文献
Weis, Simone; Shafiq, Zahid; Gropeanu, Radu A.; Del Campo, Aranzazu
Journal of Photochemistry and Photobiology A: Chemistry, 2012 , vol. 241, p. 52 - 57
反应条件
water in acetonitrile
Photolysis; Quantum yield; Wavelength;
参考文献
Bao, Chunyan; Fan, Guanshui; Lin, Qiuning; Li, Bo; Cheng, Shuiyu; Huang, Qi; Zhu, Linyong
Organic Letters, 2012 , vol. 14, # 2 p. 572 - 575
反应条件
in water
Photolysis;
参考文献
Weis, Simone; Shafiq, Zahid; Gropeanu, Radu A.; Del Campo, Aranzazu
Journal of Photochemistry and Photobiology A: Chemistry, 2012 , vol. 241, p. 52 - 57
反应条件
in N,N-dimethyl-formamide
pH=7; Photolysisaq. phosphate buffer;
参考文献
Lin, Weiying; Long, Lingliang; Tan, Wen; Chen, Bingbing; Yuan, Lin
Chemistry - A European Journal, 2010 , vol. 16, # 13 p. 3914 - 3917
反应条件
oxygen in ethanol
15 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Kalmykova, E. A.; Kuznetsova, N. A.; Kaliya, O. L.; Tavrizova, M. A.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 4.2. p. 1003 - 1010,911 - 916
反应条件
oxygen in ethanol
Irradiationvariation of concentration; MechanismQuantum yield;
参考文献
Kalmykova, E. A.; Kuznetsova, N. A.; Kaliya, O. L.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 4.2 p. 946 - 951,833 - 838
反应条件
in methanol; water
pH=7.2; UV-irradiation; Quantum yield;
参考文献
Eckardt, Torsten; Hagen, Volker; Schade, Bjoern; Schmidt, Reinhardt; Schweitzer, Claude; Bendig, Juergen
Journal of Organic Chemistry, 2002 , vol. 67, # 3 p. 703 - 710
