3-(4-溴苯基)-1,3-二苯基-1-丙酮合成路线 (共 4 条)
反应条件
1: 3,4,5-trimethoxyphenylboronic acid With diethylzinc in hexane; toluene
T=60°C; 12 h;
2: (E)-3-(4-chlorophenyl)-1-phenylprop-2-en-1-one in hexane; toluene
T=0°C; 10 h;
参考文献
Dong, Lin; Xu, Yan-Jun; Gong, Liu-Zhu; Mi, Ai-Qiao; Jiang, Yao-Zhong
Synthesis, 2004 , # 7 p. 1057 - 1061
反应条件
Rh(dpm)(CO)2; 1,3-bis(2-diphenylphosphinomethylphenyl)benzene in cyclohexane; water
T=60°C; 16 h;
参考文献
Morgan, Brad P.; Smith, Rhett C.
Journal of Organometallic Chemistry, 2008 , vol. 693, # 1 p. 11 - 16
反应条件
trifluorormethanesulfonic acid
T=25°C; 12 h;
参考文献
Rendy, Rendy; Zhang, Yun; McElrea, Aaron; Gomez, Alma; Klumpp, Douglas A.
Journal of Organic Chemistry, 2004 , vol. 69, # 7 p. 2340 - 2347
反应条件
aluminium trichloride
参考文献
Dippy; Palluel
Journal of the Chemical Society, 1951 , p. 1415,1418