3-羟基-1H-PHENALEN-1-酮合成路线 （共 24 条）
反应条件
ammonium acetate T=140 - 145°C; 2 h;
参考文献
Sawada, Tadanobu; Ishii, Hiroyuki; Aoyama, Yoshitomo; Ueda, Toyotoshi; Aoki, Junji; Takekawa, Minoru
Synthetic Communications, 2012 , vol. 42, # 6 p. 784 - 793
反应条件
1: 77 percent / diphenyl ether / 12 h / Heating 2: 30 percent / aq. NaOH / ethane-1,2-diol / 1 h / Heating View Scheme
参考文献
Stadlbauer, Wolfgang; Fischer, Michaela
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 4 p. 943 - 947
参考文献
Eistert,B. et al.
Chemische Berichte, 1968 , vol. 101, # 6 p. 2162 - 2175
反应条件
1: 51 percent / Et3N / toluene / 12 h / Heating 2: 16 percent / AlCl3 / CH2Cl2 / 12 h / Ambient temperature 3: 94 percent / POCl3, NEt3 / 1 h / Heating View Scheme
参考文献
Stadlbauer, Wolfgang; Fischer, Michaela
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 4 p. 943 - 947
反应条件
bromine; acetic acid
参考文献
Eistert,B. et al.
Chemische Berichte, 1968 , vol. 101, # 6 p. 2162 - 2175
反应条件
bromine; acetic acid
参考文献
Eistert et al.
Chemische Berichte, 1968 , vol. 101, # 6 p. 2162
反应条件
1: aq. Na2CO3
2: H2 / PtO2 / tetrahydrofuran
3: (i) aq. Br2, (ii) ascorbic acid, aq. AcOH
View Scheme
参考文献
Eistert,B. et al.
Chemische Berichte, 1968 , vol. 101, # 6 p. 2162 - 2175
反应条件
1: aq. Na2CO3
2: H2 / PtO2 / tetrahydrofuran
3: aq. Br2
View Scheme
参考文献
Eistert,B. et al.
Chemische Berichte, 1968 , vol. 101, # 6 p. 2162 - 2175
反应条件
in dimethyl sulfoxide
T=155°C; 2 h;
参考文献
Kuroki, Masatane; Terachi, Yasuhito; Tsunashima, Yutaka
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 873 - 876
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=195°C; 0.5 h;
参考文献
Kuroki, Masatane; Terachi, Yasuhito; Tsunashima, Yutaka
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 873 - 876
