3,5-二氯-4-甲基苯胺合成路线 （共 4 条）
反应条件
tin(ll) chloride in ethanol 1 h; r.t. -> 65 deg C, 20 min; 65 deg C -> r.t., 40 min;
参考文献
Banfi, Stefano; Manfredi, Amedea; Pozz, Gianluca; Quici, Silvio; Trebicka, Artan
Gazzetta Chimica Italiana, 1996 , vol. 126, # 3 p. 179 - 185
反应条件
1: 1.) SbCl5, Cl2, 2.) Cu, AcOH / 1.) H2O, 2.) PhCl 2: 81 percent / Fe, HCl / H2O View Scheme
参考文献
Tetrahedron, , vol. 54, # 12 p. 2953 - 2966
反应条件
1: iron (III)-chloride; chlorine / 60 - 70 °C / im zerstreuten Tageslicht 2: iron; hydrochloric acid View Scheme
参考文献
Journal of the Chemical Society, , vol. 121, p. 814
反应条件
1: With sodium nitrite in water T=5°C; Diazotization; 0.166667 h; 2: With copper(I) bromide T=50°C; Substitution; 0.5 h; Further stages.;
参考文献
Banfi, Stefano; Cavazzini, Marco; Pozzi, Gianluca; Barkanova, Svetlana V.; Kaliya, Oleg L.
Journal of the Chemical Society. Perkin Transactions 2, 2000 , # 4 p. 871 - 877
