苯丙氨酰-beta-丙氨酸合成路线 （共 6 条）
反应条件
hydrogen; palladium in methanol; water; acetic acid
参考文献
Ienaga; Higashiura; Kimura
Chemical and pharmaceutical bulletin, 1987 , vol. 35, # 3 p. 1249 - 1254
参考文献
Guha, Samit; Drew, Michael G. B.; Banerjee, Arindam
Organic Letters, 2007 , vol. 9, # 7 p. 1347 - 1350
反应条件
1: 90 percent / aq. NaOH / dioxane / 6 h / 20 °C
2: 90 percent / dicyclohexylcarbodiimide; 1-hydroxybenzotriazole / dimethylformamide; ethyl acetate / 72 h / 20 °C
3: 90 percent / aq. NaOH / methanol / 10 h
4: 75 percent / aq. formic acid / 8 h
View Scheme
参考文献
Guha, Samit; Drew, Michael G. B.; Banerjee, Arindam
Organic Letters, 2007 , vol. 9, # 7 p. 1347 - 1350
反应条件
1: 90 percent / dicyclohexylcarbodiimide; 1-hydroxybenzotriazole / dimethylformamide; ethyl acetate / 72 h / 20 °C
2: 90 percent / aq. NaOH / methanol / 10 h
3: 75 percent / aq. formic acid / 8 h
View Scheme
参考文献
Guha, Samit; Drew, Michael G. B.; Banerjee, Arindam
Organic Letters, 2007 , vol. 9, # 7 p. 1347 - 1350
反应条件
1: 90 percent / aq. NaOH / methanol / 10 h
2: 75 percent / aq. formic acid / 8 h
View Scheme
参考文献
Guha, Samit; Drew, Michael G. B.; Banerjee, Arindam
Organic Letters, 2007 , vol. 9, # 7 p. 1347 - 1350
反应条件
1: 82 percent / TEA / H2O; acetonitrile / 20 h / Ambient temperature
2: 88 percent / H2 / Pd / acetic acid; methanol; H2O
View Scheme
参考文献
Ienaga; Higashiura; Kimura
Chemical and pharmaceutical bulletin, 1987 , vol. 35, # 3 p. 1249 - 1254
