1-(三甲基硅氧基)-3,4-二氢苯合成路线 （共 16 条）
反应条件
oxygen O2, singlet; thiamine diphosphate in dichloromethane T=-76°C; 10 h; Product distribution;
参考文献
Clennan, Edward L.; L'Esperance, Robert P.
Tetrahedron Letters, 1983 , vol. 24, # 40 p. 4291 - 4294
反应条件
1.1: Et2Zn / diethyl ether; hexane / 0 °C
1.2: 76 percent / diethyl ether; hexane / 20 °C
2.1: 15 percent / 1,4-dicyanonaphthalene / acetonitrile / 48 h / ultrasound irradiation
View Scheme
参考文献
Rinderhagen, Heiko; Mattay, Jochen
Chemistry - A European Journal, 2004 , vol. 10, # 4 p. 851 - 874
反应条件
1: T=140°C; 6 h; Neat (no solvent);
2: With methanol; potassium carbonate
T=20°C; 0.25 h;
参考文献
Abid, Obaid-Ur-Rahman; Nawaz, Muhammad; Ibad, Muhammad Farooq; Khera, Rasheed Ahmad; Iaroshenko, Viktor; Langer, Peter
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 7 p. 2185 - 2191
反应条件
1: T=140°C; Diels-Alder reaction; 20 h;
2: With potassium carbonate in methanol
0.166667 h; Further stages.;
参考文献
Ashburn, Bradley O.; Carter, Rich G.
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 2 p. 255 - 257
反应条件
(i) MCPBA, (ii) /BRN= 385737/, Et3N*HF; Multistep reaction;
参考文献
Rubottom,G.M.; Gruber,J.M.
Journal of Organic Chemistry, 1978 , vol. 43, # 8 p. 1599 - 1602
反应条件
Yield given. Multistep reaction;
参考文献
Devasagayaraj, A.; Schwink, L.; Knochel, P.
Journal of Organic Chemistry, 1995 , vol. 60, # 11 p. 3311 - 3317
