反式-氯(1-萘)双(三苯基膦)-镍合成路线 （共 2 条）
反应条件
1: NiII chloride hexahydrate; triphenylphosphine in ethanol
T=80°C; RefluxInert atmosphere;
2: alpha-chloronaphthalene With zinc in ethanol
1 h; RefluxInert atmosphere;
3: With hydrogenchloride in ethanol; water
1.5 h;
参考文献
Mboyi, Cleve D.; Gaillard, Sylvain; Mabaye, Mbaye D.; Pannetier, Nicolas; Renaud, Jean-Luc
Tetrahedron, 2013 , vol. 69, # 24 p. 4875 - 4882
反应条件
1: With zinc in ethanol
T=65 - 70°C; 1.5 h;
2: With hydrogenchloride in ethanol; water
T=20 - 25°C; 1 h;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2009/6061 A2, 2009 ;
Location in patent: Page/Page column 28 ;
