反应条件
1: 2-bromo-N,N-bis(trimethylsilyl)aniline With n-butyllithium in diethyl ether
T=-60 - -40°C; 1 h;
2: chloro-trimethyl-silane in diethyl ether
T=-20°C;
3: With hydrogenchloride in diethyl ether
T=-7 - -5°C; Further stages.;
参考文献
Storozhenko; Belyakova; Starikova; Nosova; Shulyat'eva; Frenkel'; Pecherskii
Russian Journal of General Chemistry, 2008 , vol. 78, # 5 p. 892 - 897
