3,5-二甲基联苯-4-胺合成路线 （共 13 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethanol; toluene
48 h; Heating;
参考文献
Glende, Carsten; Schmitt, Heimo; Erdinger, Lothar; Engelhardt, Guenter; Boche, Gernot
Mutation Research - Genetic Toxicology and Environmental Mutagenesis, 2001 , vol. 498, # 1-2 p. 19 - 37
反应条件
aluminum tri-bromide
1 h; Heating;
参考文献
Takeuchi, Hiroshi; Shiobara, Yukihiko; Kawamoto, Hideyuki; Koyama, Kikuhiko
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 2 p. 321 - 327
反应条件
in water
T=250°C; 24 h;
参考文献
Mehta, Barun K.; Kumamoto, Koji; Yanagisawa, Kazumichi; Kotsuki, Hiyoshizo
Tetrahedron Letters, 2005 , vol. 46, # 40 p. 6953 - 6956
反应条件
1: 85 percent / 2,4,4,6-tetrabromocyclohexane / CH2Cl2 / 2.5 h / 20 °C
2: 39 percent / 2M Na2CO3; tetra-kis(triphenylphosphine)-palladium / toluene; ethanol / 48 h / Heating
View Scheme
参考文献
Glende, Carsten; Schmitt, Heimo; Erdinger, Lothar; Engelhardt, Guenter; Boche, Gernot
Mutation Research - Genetic Toxicology and Environmental Mutagenesis, 2001 , vol. 498, # 1-2 p. 19 - 37
反应条件
hydrogenchloride; ethanol; tin(ll) chloride
参考文献
Hey; Jackson
Journal of the Chemical Society, 1934 , p. 645,648
参考文献
I.G.Farbenind.
Patent: DE582844 , 1931 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 20, p. 449
反应条件
1: glacial acetic acid; aqueous HNO3
2: ethanol; tin (II)-chloride; aqueous hydrochloric acid
View Scheme
参考文献
Hey; Jackson
Journal of the Chemical Society, 1934 , p. 645,648
反应条件
1: aqueous potassium hypochlorite / anschliessend Behandeln mit Benzol und Aluminiumchlorid in Tetrachloraethan
2: aqueous hydrochloric acid
View Scheme
参考文献
I.G.Farbenind.
Patent: DE582844 , 1931 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 20, p. 449
反应条件
1: sulfur, quinoline
2: NO2/HNO3
3: SnCl2, aq. HCl
View Scheme
参考文献
Baker,P.B.; Saunders,B.C.
Tetrahedron, 1974 , vol. 30, p. 3303 - 3308
参考文献
Hey; Jackson
Journal of the Chemical Society, 1934 , p. 645,648
