1-[(己氧基)甲氧基]己烷合成路线 （共 8 条）
反应条件
toluene-4-sulfonic acid in toluene
36 h; Heating;
参考文献
Barot, Bhalchandra C.; Pinnick, Harold W.
Journal of Organic Chemistry, 1981 , vol. 46, # 14 p. 2981 - 2983
反应条件
1: 79 percent / diisopropylethylamine / CH2Cl2 / 12 h / Heating
2: 78 percent / p-TsOH*H2O / toluene / 36 h / Heating
View Scheme
参考文献
Barot, Bhalchandra C.; Pinnick, Harold W.
Journal of Organic Chemistry, 1981 , vol. 46, # 14 p. 2981 - 2983
反应条件
methanesulfonic acid in benzene
参考文献
Kruse,C.G. et al.
Journal of Organic Chemistry, 1978 , vol. 43, p. 3548 - 3553
反应条件
tin(IV) chloride in dichloromethane
T=0°C; 2 h; other acetal, var. times; Product distribution;
参考文献
Blumenkopf, Todd A.; Look, Gary C.; Overman, Larry E.
Journal of the American Chemical Society, 1990 , vol. 112, # 11 p. 4399 - 4403
参考文献
Vogel
Journal of the Chemical Society, 1948 , p. 631
反应条件
hydrogenchloride
Title compound not separated from byproducts;
参考文献
Pernak; Skrzypczak; Michalak; Krysinski
Die Pharmazie, 1988 , vol. 43, # 9 p. 654 - 655
反应条件
hydrogenchloride
2.) 2 h, 90 deg C; Yield given. Multistep reaction;
参考文献
Pernak; Skrzypczak; Michalak; Krysinski
Die Pharmazie, 1988 , vol. 43, # 9 p. 654 - 655
反应条件
boron trifluoride diethyl etherate
T=35°C; 5 h;
参考文献
Gazizova, L. B.; Imashev, U. B.; Musavirov, R. S.; Kantor, E. A.; Zlotskii, S. S.; et al.
Journal of Organic Chemistry USSR (English Translation), 1981 , p. 226 - 231
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 2 p. 275 - 281
