(Z)-6-二十一碳烯-11-酮合成路线 (共 124 条)
反应条件
pyridine; hydrogen; Pd-BaSO4 in methanol
参考文献
Jones, David M.; Kamijo, Shin; Dudley, Gregory B.
Synlett, 2006 , # 6 p. 936 - 938
反应条件
hydrogen; naphthalene; chromium tricarbonyl in tetrahydrofuran T=45°C; P=36775.4 Torr; 8 h;
参考文献
Sodeoka, Mikiko; Shibasaki, Masakatsu
Journal of Organic Chemistry, 1985 , vol. 50, # 7 p. 1147 - 1149
反应条件
dipyridinium dichromate in dichloromethane 41 h; Ambient temperature;
参考文献
Wenkert, Ernest; Ferreira, Vitor F.; Michelotti, Enrique L.; Tingoli, Marco
Journal of Organic Chemistry, 1985 , vol. 50, # 5 p. 719 - 721
反应条件
silica gel in tetrahydrofuran; water T=25°C; 4.5 h;
参考文献
Mitra, R. B.; Reddy, G. Bhaskar
Synthesis, 1989 , # 9 p. 694 - 698
反应条件
Amberlyst A-15 in water; acetone T=80°C; 5 h;
参考文献
Ballini, Roberto
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 6 p. 1419 - 1421
反应条件
sodium hydroxide in methanol T=80°C; 48 h;
参考文献
Muto, Shin-etsu; Mori, Kenji
Bioscience, biotechnology, and biochemistry, 2003 , vol. 67, # 7 p. 1559 - 1567
反应条件
1: nonylmagnesium chloride; N-(1-Phenylethyl)-2-methyleneaziridine With copper(l) iodide in tetrahydrofuran T=-30 - 20°C; 2: 3-cis-nonene-1-yl-p-toluenesulfonate in tetrahydrofuran T=40°C; 2 h; 3: With acetic acid in hexane T=20°C; 2 h; Further stages.;
参考文献
Hayes, Jerome F.; Shipman, Michael; Twin, Heather
Journal of Organic Chemistry, 2002 , vol. 67, # 3 p. 935 - 942
反应条件
1: tetrahydrofuran 2: pyridinium chlorochromate / CH2Cl2 View Scheme
参考文献
Bioscience, Biotechnology and Biochemistry, , vol. 69, # 5 p. 957 - 965
反应条件
1: 80 percent / tetrahydrofuran / 2 h / Heating 2: 70 percent / MnO2 / benzene / 10 h / Ambient temperature 3: 65 percent / Zn, CuI / ethanol; H2O / 0.75 h / Irradiation View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 33, # 5 p. 468 - 469
反应条件
hydrogenchloride in diethyl ether; dichloromethane 0.166667 h; Ambient temperature;
参考文献
Reddy, P. Satyanarayana; Sahasrabudhe, A. B.; Yadav, J. S.
Synthetic Communications, 1983 , vol. 13, # 5 p. 379 - 386