1: bis-o-nitrothiophenol With sodium hydride in tetrahydrofuran; mineral oil T=0°C; 0.666667 h; Inert atmosphere; 2: allyl bromide in tetrahydrofuran; mineral oil T=0 - 20°C; Inert atmosphere;

ethanol

1: sodium tetrahydroborate / tetrahydrofuran / 50 °C / |Inert atmosphere 2: potassium carbonate / N,N-dimethyl-formamide / 20 h / 20 °C / |Inert atmosphere; |Cooling with ice View Scheme

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hydrogenchloride; iron; copper dichloride