3-甲基[1,2,3]噻唑并[1,5-a]吡啶合成路线 （共 32 条）
反应条件
1: With polystyrene-sulfonyl hydrazide resin; titanium tetrachloride in methanol; dichloromethane T=20°C; 12 h; 2: With morpholine T=95°C; 4 h; Further stages.;
参考文献
Raghavendra, Makam S.; Lam, Yulin
Tetrahedron Letters, 2004 , vol. 45, # 32 p. 6129 - 6132
反应条件
tetrakis(triphenylphosphine) palladium(0); para-iodoanisole; potassium carbonate in ethylene glycol dimethyl ether T=80°C;
参考文献
Abarca, Belen; Ballesteros, Rafael; Blanco, Fernando; Bouillon, Alexandre; Collot, Valerie; Dominguez, Jose-Reynaldo; Lancelot, Jean-Charles; Rault, Sylvain
Tetrahedron, 2004 , vol. 60, # 22 p. 4887 - 4893
反应条件
[bis(acetoxy)iodo]benzene in dichloromethane T=20°C; Cyclization; 0.5 h;
参考文献
Prakash, Om; Gujral, Harpreet K.; Rani, Neena; Singh, Shiv P.
Synthetic Communications, 2000 , vol. 30, # 3 p. 417 - 425
反应条件
palladium diacetate; caesium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=140°C; 2 h; Inert atmosphere;
参考文献
Abarca, Belen; Adam, Rosa; Ballesteros, Rafael; Chiassai, Leonardo; Gamon, Cristina
Arkivoc, 2012 , vol. 2012, # 9 p. 229 - 241
反应条件
barium dihydroxide; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=50 - 60°C; Suzuki cross-coupling reaction; 72 h;
参考文献
Tetrahedron, , vol. 60, # 22 p. 4887 - 4893
反应条件
barium dihydroxide; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=90 - 100°C; Suzuki cross-coupling reaction; 20 h;
参考文献
Tetrahedron, , vol. 60, # 22 p. 4887 - 4893
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=70°C; Suzuki cross-coupling reaction; 16 h;
参考文献
Tetrahedron, , vol. 60, # 22 p. 4887 - 4893
反应条件
copper(l) iodide; palladium diacetate; caesium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=140°C; 2 h; Inert atmosphere;
参考文献
Arkivoc, , vol. 2012, # 9 p. 229 - 241
反应条件
barium dihydroxide; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=80 - 100°C; Suzuki cross-coupling reaction; 24 h;
参考文献
Tetrahedron, , vol. 60, # 22 p. 4887 - 4893
反应条件
barium dihydroxide; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=90 - 100°C; Suzuki cross-coupling reaction; 20 h;
参考文献
Tetrahedron, , vol. 60, # 22 p. 4887 - 4893
