乙基5-甲基-4-氧代己酸酯合成路线 （共 12 条）
反应条件
1: diiodomethane With diethylzinc; trifluoroacetic acid in dichloromethane 0.5 h; 2: 4-methyl-3-oxo-pentanoic acid ethyl ester in dichloromethane T=20°C; 8 h;
参考文献
Journal of Organic Chemistry, , vol. 70, # 20 p. 8245 - 8247
反应条件
1: 90 percent / acetonitrile; various solvent(s) / Irradiation; 300 nm 2: p-toluenesulfonic acid / benzene / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 23, # 4 p. 481 - 484
反应条件
toluene-4-sulfonic acid in benzene Heating; Yield given;
参考文献
Tetrahedron Letters, , vol. 23, # 4 p. 481 - 484
反应条件
(i), (ii) (hydrolysis); Multistep reaction;
参考文献
Tetrahedron Letters, , p. 341 - 344
反应条件
sulfuric acid T=20°C;
参考文献
Guijarro, David; Pablo, Oscar; Yus, Miguel
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3647 - 3654
反应条件
1: 1.) lithium-diisopropylamide, 2.) HMPT, LiBr / 1.) THF, hexane, 2.) -78 deg C, 30 min, THF 2: 25percent CuSO4 / 40 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 8 p. 645 - 647
参考文献
Journal of the Chemical Society, , p. 583
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 30, p. 1000 - 1001
参考文献
Bulletin de la Societe Chimique de France, , vol. <5> 4, p. 1658,1659
反应条件
in acetone Irradiation300 nm;
参考文献
Tetrahedron Letters, , vol. 23, # 4 p. 481 - 484
