6-氯-N,N-二乙基-3-吡啶磺酰胺合成路线 （共 3 条）
参考文献
Naegeli et al.
Helvetica Chimica Acta, 1939 , vol. 22, p. 912,920
反应条件
1.1: n-butyllithium; Di-n-butylmagnesium / tetrahydrofuran / -10 °C / Inert atmosphere
1.2: -10 - 10 °C
2.1: tetrahydrofuran; toluene / 0.5 h / 10 °C
View Scheme
参考文献
Emura, Takashi; Yoshino, Hitoshi; Tachibana, Kazutaka; Shiraishi, Takuya; Honma, Akie; Mizutani, Akemi; Muraoka, Terushige
Synlett, 2011 , # 8 art. no. U00411ST, p. 1117 - 1120
反应条件
ammonium hydroxide
T=145°C;
参考文献
Naegeli et al.
Helvetica Chimica Acta, 1942 , vol. 25, p. 1485,1492
