反应条件
1: pyridine / 2 h / 0 °C
2: 40 mg / dimethylsulfoxide / 7 h / 60 °C
3: 96 percent / 1.5 M aq. perchloric acid / tetrahydrofuran / 1 h / 0 °C
4: diethyl ether / 1 h / 0 °C
5: 1.) methanesulfonyl chloride / 1.) pyridine, 1 h, 2.) dimethyl sulfoxide, 50-60 deg C, 1 h
View Scheme
参考文献
White, James D.; Ruppert, John F.; Avery, Mitchell A.; Torii, Sigeru; Nokami, Junzo
Journal of the American Chemical Society, 1981 , vol. 103, # 7 p. 1813 - 1821
