4-溴-N,N-双(4-丁基苯基)-苯胺合成路线 （共 6 条）
反应条件
1: NBS / CCl4 / Heating
2: tetrahydrofuran; hexane / 0.75 h / -78 °C
View Scheme
参考文献
Zhang, Hongyu; Huo, Cheng; Zhang, Jingying; Zhang, Peng; Tian, Wenjing; Wang, Yue
Chemical Communications, 2006 , # 3 p. 281 - 283
反应条件
polyethylene glycol; copper bronze; potassium carbonate in 1,2-dichloro-benzene
Heating;
参考文献
Luo, Qianfu; Sheng, Saihong; Cheng, Saihe; Tian, He
Australian Journal of Chemistry, 2005 , vol. 58, # 5 p. 321 - 326
反应条件
in tetrahydrofuran; hexane
T=-78°C; 0.75 h;
参考文献
Zhang, Hongyu; Huo, Cheng; Zhang, Jingying; Zhang, Peng; Tian, Wenjing; Wang, Yue
Chemical Communications, 2006 , # 3 p. 281 - 283
反应条件
1.1: HCl; NaNO2 / 5 °C
1.2: KI / H2O / 5 °C
2.1: 40 percent / K2CO3; bronze powder; polyethylene glycol / 1,2-dichloro-benzene / Heating
View Scheme
参考文献
Luo, Qianfu; Sheng, Saihong; Cheng, Saihe; Tian, He
Australian Journal of Chemistry, 2005 , vol. 58, # 5 p. 321 - 326
反应条件
1: tris-(dibenzylideneacetone)dipalladium(0); HP-t-Bu3BF4; sodium t-butanolate / toluene
2: N-bromosuccinmide / dichloromethane
View Scheme
参考文献
Kamtekar, Kiran T.; Dahms, Katja; Batsanov, Andrei S.; Jankus, Vygintas; Vaughan, Helen L.; Monkman, Andrew P.; Bryce, Martin R.
Journal of Polymer Science, Part A: Polymer Chemistry, 2011 , vol. 49, # 5 p. 1129 - 1137
反应条件
1: tris-(dibenzylideneacetone)dipalladium(0); HP-t-Bu3BF4; sodium t-butanolate / toluene
2: N-bromosuccinmide / dichloromethane
View Scheme
参考文献
Kamtekar, Kiran T.; Dahms, Katja; Batsanov, Andrei S.; Jankus, Vygintas; Vaughan, Helen L.; Monkman, Andrew P.; Bryce, Martin R.
Journal of Polymer Science, Part A: Polymer Chemistry, 2011 , vol. 49, # 5 p. 1129 - 1137
